C₁₅H₁₃BrF₃NO

Base Information

Chemical Name:C₁₅H₁₃BrF₃NO
CAS No.:1160359-92-1
Molecular Formula:C₁₅H₁₃BrF₃NO
Molecular Weight:360.174
Hs Code.:

C<sub>15</sub>H<sub>13</sub>BrF<sub>3</sub>NO

Synonyms:C₁₅H₁₃BrF₃NO

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Chemical Property of C₁₅H₁₃BrF₃NO

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Technology Process of C₁₅H₁₃BrF₃NO

There total 9 articles about C₁₅H₁₃BrF₃NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1160359-91-0
C₁₅H₁₃BrFNO₂

: 1160359-92-1
C₁₅H₁₃BrF₃NO

Guidance literature:: With (bis-(2-methoxyethyl)amino)sulfur trufluoride; In tetrahydrofuran; at 80 ℃; for 48h; Inert atmosphere; Sealed tube;
DOI:10.1021/ml2000438

Reference yield:

: 1128105-86-1
C₁₅H₁₃BrFNO₃

: 1160359-92-1
C₁₅H₁₃BrF₃NO

Guidance literature:: Multi-step reaction with 7 steps

1: water; sodium hydroxide / methanol / 16 h / 20 °C / Inert atmosphere

2: pyridine; trifluoro-[1,3,5]triazine / dichloromethane / -10 - 20 °C / Inert atmosphere

3: sodium tetrahydroborate / methanol; dichloromethane / 2 h / 20 °C / Inert atmosphere

4: dipyridinium dichromate / dichloromethane / 4 h / 20 °C / Inert atmosphere

5: tetrahydrofuran; diethyl ether / 2 h / -78 °C / Inert atmosphere

6: dipyridinium dichromate / dichloromethane / 16 h / 20 °C / Inert atmosphere

7: (bis-(2-methoxyethyl)amino)sulfur trufluoride / tetrahydrofuran / 48 h / 80 °C / Inert atmosphere; Sealed tube

With pyridine; sodium tetrahydroborate; dipyridinium dichromate; trifluoro-[1,3,5]triazine; water; sodium hydroxide; (bis-(2-methoxyethyl)amino)sulfur trufluoride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;
DOI:10.1021/ml2000438

Reference yield:

: 1128105-87-2
C₁₄H₁₃BrFNO₂

: 1160359-92-1
C₁₅H₁₃BrF₃NO

Guidance literature:: Multi-step reaction with 4 steps

1: dipyridinium dichromate / dichloromethane / 4 h / 20 °C / Inert atmosphere

2: tetrahydrofuran; diethyl ether / 2 h / -78 °C / Inert atmosphere

3: dipyridinium dichromate / dichloromethane / 16 h / 20 °C / Inert atmosphere

4: (bis-(2-methoxyethyl)amino)sulfur trufluoride / tetrahydrofuran / 48 h / 80 °C / Inert atmosphere; Sealed tube

With dipyridinium dichromate; (bis-(2-methoxyethyl)amino)sulfur trufluoride; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/ml2000438