α-naphthalen-2-ylacrylic acid

Base Information

Chemical Name:α-naphthalen-2-ylacrylic acid
CAS No.:75029-76-4
Molecular Formula:C₁₃H₁₀O₂
Molecular Weight:198.221
Hs Code.:

Synonyms:α-naphthalen-2-ylacrylic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α-naphthalen-2-ylacrylic acid

Chemical Property:

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Technology Process of α-naphthalen-2-ylacrylic acid

There total 1 articles about α-naphthalen-2-ylacrylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21473-01-8
2-naphthalenylmagnesium bromide

: 75029-76-4
α-naphthalen-2-ylacrylic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 1 h / -78 °C / Schlenk technique; Inert atmosphere

2.1: potassium hexamethylsilazane / tetrahydrofuran / 1.25 h / -78 - 20 °C / Inert atmosphere; Schlenk technique

2.2: 1 h / -78 °C / Inert atmosphere; Schlenk technique

3.1: lithium hydroxide / tetrahydrofuran; water / 80 °C / Schlenk technique

With potassium hexamethylsilazane; lithium hydroxide; In tetrahydrofuran; water;
DOI:10.1002/anie.201307245

Reference yield: 92.0%

: 12354-84-6,12354-85-7
bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]

: 75029-76-4
α-naphthalen-2-ylacrylic acid

: 501-65-5
diphenyl acetylene

: C₃₇H₃₃IrO₂

Guidance literature:: With tetrabutylammonium acetate; In methanol; at 60 ℃; for 12h;
DOI:10.1021/jacs.9b11915

Reference yield: 91.0%

: 75029-76-4
α-naphthalen-2-ylacrylic acid

: 501-65-5
diphenyl acetylene

: 3-(naphthalen-2-yl)-5,6-diphenyl-2H-pyran-2-one

Guidance literature:: With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; tetrabutylammonium acetate; In methanol; at 60 ℃; for 12h; Electrochemical reaction;
DOI:10.1021/jacs.9b11915