Technology Process of C41H19F15N4
There total 3 articles about C41H19F15N4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 20 ℃;
for 1.5h;
Inert atmosphere;
DOI:10.1002/anie.201203712
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: trifluoroacetic acid / 2.17 h / 20 °C / Inert atmosphere
2.1: ethylmagnesium bromide / tetrahydrofuran / 0.35 h / 20 °C / Inert atmosphere
2.2: -78 - 20 °C / Inert atmosphere
3.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 0 - 20 °C / Inert atmosphere
4.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C / Inert atmosphere
5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere
With
sodium tetrahydroborate; ethylmagnesium bromide; tetrabutyl ammonium fluoride; trifluoroacetic acid;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/anie.201203712
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: ethylmagnesium bromide / tetrahydrofuran / 0.35 h / 20 °C / Inert atmosphere
1.2: -78 - 20 °C / Inert atmosphere
2.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 0 - 20 °C / Inert atmosphere
3.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C / Inert atmosphere
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere
With
sodium tetrahydroborate; ethylmagnesium bromide; tetrabutyl ammonium fluoride; trifluoroacetic acid;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/anie.201203712