C₅₅H₈₆O₁₁Si₂

Base Information

Chemical Name:C₅₅H₈₆O₁₁Si₂
CAS No.:1283735-80-7
Molecular Formula:C₅₅H₈₆O₁₁Si₂
Molecular Weight:979.452
Hs Code.:

C<sub>55</sub>H<sub>86</sub>O<sub>11</sub>Si<sub>2</sub>

Synonyms:C₅₅H₈₆O₁₁Si₂

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Chemical Property of C₅₅H₈₆O₁₁Si₂

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Technology Process of C₅₅H₈₆O₁₁Si₂

There total 23 articles about C₅₅H₈₆O₁₁Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₅H₈₄O₁₀Si₂

: 1283735-80-7
C₅₅H₈₆O₁₁Si₂

Guidance literature:: With acetic acid; zinc; In tetrahydrofuran; at 20 ℃; for 10h;
DOI:10.1002/asia.201000882

Reference yield:

: 1202748-08-0
C₂₈H₃₆O₄Si

: 1283735-80-7
C₅₅H₈₆O₁₁Si₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: ammonium cerium (IV) nitrate; sodium hydrogencarbonate / water; acetonitrile / 0.17 h / 0 °C

2.1: 1H-imidazole; dmap / 0 - 20 °C

3.1: pyridinium p-toluenesulfonate / methanol; dichloromethane / 6 h / 0 °C

4.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 0 °C

5.1: n-butyllithium / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

5.2: -78 - 20 °C

6.1: bis-[(trifluoroacetoxy)iodo]benzene; calcium carbonate / dichloromethane; water; acetonitrile / 0.17 h / 0 °C

7.1: dmap; triethylamine / dichloromethane / 20 °C

8.1: oxygen; 5,15,10,20-tetraphenylporphyrin / dichloromethane / 3 h / -78 °C / UV-irradiation

9.1: acetic acid; zinc / tetrahydrofuran / 10 h / 20 °C

With 1H-imidazole; dmap; n-butyllithium; ammonium cerium (IV) nitrate; oxygen; pyridinium p-toluenesulfonate; 5,15,10,20-tetraphenylporphyrin; sodium hydrogencarbonate; Dess-Martin periodane; acetic acid; triethylamine; bis-[(trifluoroacetoxy)iodo]benzene; calcium carbonate; zinc; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;
DOI:10.1002/asia.201000882

Reference yield:

: 415916-72-2
C₂₆H₄₂O₆

: 1283735-80-7
C₅₅H₈₆O₁₁Si₂

Guidance literature:: Multi-step reaction with 12 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 - 20 °C

2.1: pyridine; dmap / 5 h / 0 °C

3.1: pyridine; methanesulfonyl chloride / 5 h / 0 - 55 °C

4.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); cyclohexane-1,2-epoxide / tetrachloromethane / 10 h / 90 °C

5.1: methanol; potassium carbonate / 20 °C

6.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 2 h / 0 °C

7.1: toluene-4-sulfonic acid / dichloromethane / 4 h / 0 °C

8.1: n-butyllithium / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

8.2: -78 - 20 °C

9.1: bis-[(trifluoroacetoxy)iodo]benzene; calcium carbonate / dichloromethane; water; acetonitrile / 0.17 h / 0 °C

10.1: dmap; triethylamine / dichloromethane / 20 °C

11.1: oxygen; 5,15,10,20-tetraphenylporphyrin / dichloromethane / 3 h / -78 °C / UV-irradiation

12.1: acetic acid; zinc / tetrahydrofuran / 10 h / 20 °C

With pyridine; methanol; dmap; N-Bromosuccinimide; lithium aluminium tetrahydride; n-butyllithium; 2,2'-azobis(isobutyronitrile); oxygen; 5,15,10,20-tetraphenylporphyrin; cyclohexane-1,2-epoxide; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; toluene-4-sulfonic acid; acetic acid; methanesulfonyl chloride; triethylamine; bis-[(trifluoroacetoxy)iodo]benzene; calcium carbonate; zinc; In tetrahydrofuran; tetrachloromethane; dichloromethane; water; acetonitrile;
DOI:10.1002/asia.201000882