N-hydroxy-4-{[(3,4-dimethoxyphenylcarbamoylmethyl)amino]methyl}benzamide

Base Information

Chemical Name:N-hydroxy-4-{[(3,4-dimethoxyphenylcarbamoylmethyl)amino]methyl}benzamide
CAS No.:1393643-89-4
Molecular Formula:C₁₈H₂₁N₃O₅
Molecular Weight:359.382
Hs Code.:

Synonyms:N-hydroxy-4-{[(3,4-dimethoxyphenylcarbamoylmethyl)amino]methyl}benzamide

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Chemical Property of N-hydroxy-4-{[(3,4-dimethoxyphenylcarbamoylmethyl)amino]methyl}benzamide

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Technology Process of N-hydroxy-4-{[(3,4-dimethoxyphenylcarbamoylmethyl)amino]methyl}benzamide

There total 4 articles about N-hydroxy-4-{[(3,4-dimethoxyphenylcarbamoylmethyl)amino]methyl}benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.3%

: C₁₉H₂₂N₂O₅

: 1393643-89-4
N-hydroxy-4-{[(3,4-dimethoxyphenylcarbamoylmethyl)amino]methyl}benzamide

Guidance literature:: With hydroxylamine hydrochloride; sodium hydroxide; In methanol; water; at 20 ℃;
DOI:10.3390/molecules16119178

Reference yield:

: 6315-89-5
3,4-dimethoxyaniline

: 1393643-89-4
N-hydroxy-4-{[(3,4-dimethoxyphenylcarbamoylmethyl)amino]methyl}benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / -5 - 20 °C

2: potassium hydrogencarbonate / acetonitrile / Reflux

3: hydroxylamine hydrochloride; sodium hydroxide / methanol; water / 20 °C

With hydroxylamine hydrochloride; potassium hydrogencarbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In methanol; dichloromethane; water; acetonitrile;
DOI:10.3390/molecules16119178

Reference yield:

: 6232-11-7
methyl 4-(aminomethyl)benzoate hydrochloride

: 1019399-51-9
2-bromo-N-(3,4-dimethoxy-phenyl)-acetamide

: 1393643-89-4
N-hydroxy-4-{[(3,4-dimethoxyphenylcarbamoylmethyl)amino]methyl}benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydrogencarbonate / acetonitrile / Reflux

2: hydroxylamine hydrochloride; sodium hydroxide / methanol; water / 20 °C

With hydroxylamine hydrochloride; potassium hydrogencarbonate; sodium hydroxide; In methanol; water; acetonitrile;
DOI:10.3390/molecules16119178