di-tert-butyl ethane-1,2-diylbis((3-((4-((E)-phenyldiazenyl)benzyl)amino)propyl)carbamate)

Base Information

• Chemical Name: di-tert-butyl ethane-1,2-diylbis((3-((4-((E)-phenyldiazenyl)benzyl)amino)propyl)carbamate)
• CAS No.: 1610930-01-2
• Molecular Formula: C₄₄H₅₈N₈O₄
• Molecular Weight: 762.996

Synonyms:di-tert-butyl ethane-1,2-diylbis((3-((4-((E)-phenyldiazenyl)benzyl)amino)propyl)carbamate)

Chemical Property of di-tert-butyl ethane-1,2-diylbis((3-((4-((E)-phenyldiazenyl)benzyl)amino)propyl)carbamate)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of di-tert-butyl ethane-1,2-diylbis((3-((4-((E)-phenyldiazenyl)benzyl)amino)propyl)carbamate)

There total 8 articles about di-tert-butyl ethane-1,2-diylbis((3-((4-((E)-phenyldiazenyl)benzyl)amino)propyl)carbamate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C44H54N8O4 (1629797-24-5) → di-tert-butyl ethane-1,2-diylbis((3-((4-((E)-phenyldiazenyl)benzyl)amino)propyl)carbamate) (1610930-01-2)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 20 ℃; Inert atmosphere;

DOI:10.1002/chem.201304658

Reference yield:

2,2,2-Trifluoro-N-(3-{2-[3-(2,2,2-trifluoro-acetylamino)-propylamino]-ethylamino}-propyl)-acetamide (181181-34-0) → di-tert-butyl ethane-1,2-diylbis((3-((4-((E)-phenyldiazenyl)benzyl)amino)propyl)carbamate) (1610930-01-2)

Guidance literature:

Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 20 °C / Inert atmosphere

2: sodium hydroxide; water / ethanol / 20 °C / Inert atmosphere

3: ethanol / 24 h / Reflux; Molecular sieve; Inert atmosphere

4: sodium tetrahydroborate / methanol / 20 °C / Inert atmosphere

With sodium tetrahydroborate; water; triethylamine; sodium hydroxide; In methanol; ethanol; dichloromethane;

DOI:10.1002/chem.201304658

Reference yield:

(E)-(4-(phenyldiazenyl)phenyl)methanol (65926-74-1) → di-tert-butyl ethane-1,2-diylbis((3-((4-((E)-phenyldiazenyl)benzyl)amino)propyl)carbamate) (1610930-01-2)

Guidance literature:

Multi-step reaction with 3 steps

1: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

2: ethanol / 24 h / Reflux; Molecular sieve; Inert atmosphere

3: sodium tetrahydroborate / methanol / 20 °C / Inert atmosphere

With sodium tetrahydroborate; Dess-Martin periodane; In methanol; ethanol; dichloromethane;

DOI:10.1002/chem.201304658

upstream raw materials:

N,N'-bis(3-aminopropyl)-1,2-diamine

2,2,2-Trifluoro-N-(3-{2-[3-(2,2,2-trifluoro-acetylamino)-propylamino]-ethylamino}-propyl)-acetamide

(E)-4-(phenyldiazenyl)benzoic acid

N,N'-(ethylenebis{[(tert-butoxycarbonyl)imino]propane-1,3-diyl})bis(trifluoroacetamide)

Downstream raw materials:

N¹,N^1'-(ethane-1,2-diyl)bis(N³-(4-((E)-phenyldiazenyl)benzyl)propane-1,3-diamine)

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1610930-01-2 di-tert-butyl ethane-1,2-diylbis((3-((4-((E)-phenyldiazenyl)benzyl)amino)propyl)carbamate)

Send

Send

Metric Ton KG G Pound L ML

Send

Send