C₂₂H₃₂N₄O₅

Base Information

Chemical Name:C₂₂H₃₂N₄O₅
CAS No.:1221447-95-5
Molecular Formula:C₂₂H₃₂N₄O₅
Molecular Weight:432.52
Hs Code.:

C<sub>22</sub>H<sub>32</sub>N<sub>4</sub>O<sub>5</sub>

Synonyms:C₂₂H₃₂N₄O₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₃₂N₄O₅

Chemical Property:

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Technology Process of C₂₂H₃₂N₄O₅

There total 8 articles about C₂₂H₃₂N₄O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1221447-93-3
C₂₂H₃₀N₄O₇

: 1221447-95-5
C₂₂H₃₂N₄O₅

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In methanol; at 20 ℃; for 4h;

Reference yield:

: 82685-82-3
C₁₀H₉NO₄

: 1221447-95-5
C₂₂H₃₂N₄O₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C

1.2: 0.5 h

2.1: potassium carbonate / tetrahydrofuran / 2 h / -68 - -65 °C / Inert atmosphere

2.2: 4 h / -65 °C

3.1: N,N-dimethyl-formamide / 20 °C

4.1: ammonium cerium (IV) nitrate / acetonitrile; water / 4 h / 20 - 85 °C

5.1: dmap / dichloromethane; tetrahydrofuran / 0.75 h / 20 °C

6.1: hydrogen / palladium 10% on activated carbon / methanol / 4 h / 20 °C

With ammonium cerium (IV) nitrate; oxalyl dichloride; hydrogen; potassium carbonate; dmap; palladium 10% on activated carbon; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1221447-91-1
C₂₀H₂₂N₄O₄

: 1221447-95-5
C₂₂H₃₂N₄O₅

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium cerium (IV) nitrate / acetonitrile; water / 4 h / 20 - 85 °C

2: dmap / dichloromethane; tetrahydrofuran / 0.75 h / 20 °C

3: hydrogen / palladium 10% on activated carbon / methanol / 4 h / 20 °C

With ammonium cerium (IV) nitrate; hydrogen; dmap; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;