3--1-cyclohexenecarboxylic acid methyl ester

Base Information

Chemical Name:3--1-cyclohexenecarboxylic acid methyl ester
CAS No.:106093-98-5
Molecular Formula:C₁₃H₁₈O₇
Molecular Weight:286.282
Hs Code.:

3-<bis(methoxycarbonyl)methoxy>-1-cyclohexenecarboxylic acid methyl ester

Synonyms:3--1-cyclohexenecarboxylic acid methyl ester

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Chemical Property of 3--1-cyclohexenecarboxylic acid methyl ester

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Technology Process of 3--1-cyclohexenecarboxylic acid methyl ester

There total 4 articles about 3--1-cyclohexenecarboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 6773-29-1
dimethyl diazomalonate

: 106093-97-4,122620-80-8,134529-74-1
3-hydroxy-1-cyclohexenecarboxylic acid methyl ester

: 106093-98-5
3--1-cyclohexenecarboxylic acid methyl ester

Guidance literature:: With rhodium(II) acetate; In benzene; for 0.583333h; Heating;
DOI:10.1021/ja00238a029

Reference yield:

: endo-8-bromo-6-oxabicyclo<3.2.1>octa-2-en-7-one

: 106093-98-5
3--1-cyclohexenecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / hydrogen / 10percent Pd/C / ethanol / 6 h

2: 68 percent / methanol / 18 h

3: 95 percent / rhodium acetate / benzene / 0.58 h / Heating

With rhodium(II) acetate; hydrogen; palladium on activated charcoal; In methanol; ethanol; benzene;
DOI:10.1021/ja00238a029

Reference yield:

: endo-8-bromo-6-oxabicyclo<3.2.1>octa-7-one

: 106093-98-5
3--1-cyclohexenecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / methanol / 18 h

2: 95 percent / rhodium acetate / benzene / 0.58 h / Heating

With rhodium(II) acetate; In methanol; benzene;
DOI:10.1021/ja00238a029