(((CH₃)2CH)2C₆H₃NC(CH₃))(O₂CH₂)C₆H₂GeCl

Base Information

• Chemical Name: (((CH₃)2CH)2C₆H₃NC(CH₃))(O₂CH₂)C₆H₂GeCl
• CAS No.: 1352569-33-5
• Molecular Formula: C₂₁H₂₄ClGeNO₂
• Molecular Weight: 430.47

Synonyms:(((CH₃)2CH)2C₆H₃NC(CH₃))(O₂CH₂)C₆H₂GeCl

Chemical Property of (((CH₃)2CH)2C₆H₃NC(CH₃))(O₂CH₂)C₆H₂GeCl

Chemical Property:

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Technology Process of (((CH₃)2CH)2C₆H₃NC(CH₃))(O₂CH₂)C₆H₂GeCl

There total 1 articles about (((CH₃)2CH)2C₆H₃NC(CH₃))(O₂CH₂)C₆H₂GeCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.4%

germanium(II) chloride dioxane + Li(1+)*CH2O2C6H2CCH3NC6H3(CH(CH3)2)2(1-)=LiCH2O2C6H2CCH3NC6H3(CH(CH3)2)2 → (((CH3)2CH)2C6H3NC(CH3))(O2CH2)C6H2GeCl (1352569-33-5)

Guidance literature:

In diethyl ether; (Ar) soln. aryllithium in Et2O was added at 0°C to suspn. Ge complex in Et2O, warmed to room temp., stirred for 15 h; soln. was filtered and concd.; elem. anal.;

DOI:10.1021/ic202138t

Reference yield: 70.5%

(((CH3)2CH)2C6H3NC(CH3))(O2CH2)C6H2GeCl (1352569-33-5) → ((((CH3)2CH)2C6H3NC(CH3))(O2CH2)C6H2Ge)2 (1352569-34-6)

Guidance literature:

With KC₈; In tetrahydrofuran; (Ar) THF was added to mixt. Ge complex and KC8 at room temp., stirred overnight; soln. was filtered, volatiles were removed in vacuo, residue was extd. with Et2O, filtered and concd.; elem. anal.;

DOI:10.1021/ic202138t

Reference yield: 43.5%

potassium graphite + (((CH3)2CH)2C6H3NC(CH3))(O2CH2)C6H2GeCl (1352569-33-5) → K(1+)*((((CH3)2CH)2C6H3NC(CH3))(O2CH2)C6H2Ge)(1-)=(((CH3)2CH)2C6H3NC(CH3))(O2CH2)C6H2GeK

Guidance literature:

In tetrahydrofuran; (Ar) THF was added at room temp. to mixt. Ge complex and KC8, stirred overnight; soln. was filtered, volatiles were removed in vacuo, residue was extd. with Et2O, filtered and concd.; elem. anal.;

DOI:10.1021/ic202138t

Downstream raw materials:

((((CH₃)2CH)2C₆H₃NC(CH₃))(O₂CH₂)C₆H₂Ge)2

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