1,1-dimethylethyl {3,5-bis{{[(1,1-dimethylethyl)dimethylsilyl]oxy}methyl}phenoxy}acetate

Base Information

Chemical Name:1,1-dimethylethyl {3,5-bis{{[(1,1-dimethylethyl)dimethylsilyl]oxy}methyl}phenoxy}acetate
CAS No.:434929-00-7
Molecular Formula:C₂₆H₄₈O₅Si₂
Molecular Weight:496.835
Hs Code.:

Synonyms:1,1-dimethylethyl {3,5-bis{{[(1,1-dimethylethyl)dimethylsilyl]oxy}methyl}phenoxy}acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1-dimethylethyl {3,5-bis{{[(1,1-dimethylethyl)dimethylsilyl]oxy}methyl}phenoxy}acetate

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Technology Process of 1,1-dimethylethyl {3,5-bis{{[(1,1-dimethylethyl)dimethylsilyl]oxy}methyl}phenoxy}acetate

There total 5 articles about 1,1-dimethylethyl {3,5-bis{{[(1,1-dimethylethyl)dimethylsilyl]oxy}methyl}phenoxy}acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 5292-43-3
bromoacetic acid tert-butyl ester

: 434928-99-1
3,5-bis{{[(1,1-dimethylethyl)dimethylsilyl]oxy}methyl}phenol

: 434929-00-7
1,1-dimethylethyl {3,5-bis{{[(1,1-dimethylethyl)dimethylsilyl]oxy}methyl}phenoxy}acetate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 72h;
DOI:10.1002/1522-2675(200201)85:1<288::AID-HLCA288>3.0.CO;2-I

Reference yield:

: 13036-02-7
Dimethyl 5-hydroxyisophthalate

: 434929-00-7
1,1-dimethylethyl {3,5-bis{{[(1,1-dimethylethyl)dimethylsilyl]oxy}methyl}phenoxy}acetate

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / 1H-imidazole / dimethylformamide / 3 h / 0 °C

2: 97 percent / LiAlH₄ / tetrahydrofuran / 5 h / 0 °C

3: 85 percent / 1H-imidazole / dimethylformamide / 3 h / 0 °C

4: 88 percent / Bu₄NF / tetrahydrofuran / 0.25 h / 0 °C

5: 95 percent / K₂CO₃ / dimethylformamide / 72 h / 80 °C

With 1H-imidazole; lithium aluminium tetrahydride; tetrabutyl ammonium fluoride; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/1522-2675(200201)85:1<288::AID-HLCA288>3.0.CO;2-I

Reference yield:

: 182629-25-0
5-{[(1,1-dimethylethyl)dimethylsilyl]oxy}benzene-1,3-dimethanol

: 434929-00-7
1,1-dimethylethyl {3,5-bis{{[(1,1-dimethylethyl)dimethylsilyl]oxy}methyl}phenoxy}acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / 1H-imidazole / dimethylformamide / 3 h / 0 °C

2: 88 percent / Bu₄NF / tetrahydrofuran / 0.25 h / 0 °C

3: 95 percent / K₂CO₃ / dimethylformamide / 72 h / 80 °C

With 1H-imidazole; tetrabutyl ammonium fluoride; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/1522-2675(200201)85:1<288::AID-HLCA288>3.0.CO;2-I