1-[1-((E)-1-Methoxy-3-phenyl-allyl)-cyclopentyl]-3-trimethylsilanyl-propynone

Base Information

Chemical Name:1-[1-((E)-1-Methoxy-3-phenyl-allyl)-cyclopentyl]-3-trimethylsilanyl-propynone
CAS No.:123474-80-6
Molecular Formula:C₂₁H₂₈O₂Si
Molecular Weight:340.538
Hs Code.:

Synonyms:1-[1-((E)-1-Methoxy-3-phenyl-allyl)-cyclopentyl]-3-trimethylsilanyl-propynone

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Chemical Property of 1-[1-((E)-1-Methoxy-3-phenyl-allyl)-cyclopentyl]-3-trimethylsilanyl-propynone

Chemical Property:

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Technology Process of 1-[1-((E)-1-Methoxy-3-phenyl-allyl)-cyclopentyl]-3-trimethylsilanyl-propynone

There total 9 articles about 1-[1-((E)-1-Methoxy-3-phenyl-allyl)-cyclopentyl]-3-trimethylsilanyl-propynone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 123475-03-6
1-[1-((E)-1-Methoxy-3-phenyl-allyl)-cyclopentyl]-3-trimethylsilanyl-prop-2-yn-1-ol

: 123474-80-6
1-[1-((E)-1-Methoxy-3-phenyl-allyl)-cyclopentyl]-3-trimethylsilanyl-propynone

Guidance literature:: With manganese(IV) oxide; In dichloromethane;
DOI:10.1016/S0040-4039(01)80627-4

Reference yield:

: 28247-15-6
ethyl 1-acetylcyclopropane-1-carboxylate

: 123474-80-6
1-[1-((E)-1-Methoxy-3-phenyl-allyl)-cyclopentyl]-3-trimethylsilanyl-propynone

Guidance literature:: Multi-step reaction with 7 steps

1: 40 percent / LDA / tetrahydrofuran

2: 95 percent / NaBH₄-CeCl₃*7H₂O / methanol

3: 93 percent / NaH / dimethylformamide

4: 99 percent / DIBAL-H / tetrahydrofuran

5: 95 percent / SO₃*Py, Et₃N / dimethylsulfoxide

6: 98 percent

7: 96 percent / MnO₂ / CH₂Cl₂

With manganese(IV) oxide; sodium tetrahydroborate; cerium(III) chloride; pyridine-SO₃ complex; sodium hydride; diisobutylaluminium hydride; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(01)80627-4

Reference yield:

: 54655-07-1
lithium trimethylsilylacetylenide

: 123474-80-6
1-[1-((E)-1-Methoxy-3-phenyl-allyl)-cyclopentyl]-3-trimethylsilanyl-propynone

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent

2: 96 percent / MnO₂ / CH₂Cl₂

With manganese(IV) oxide; In dichloromethane;
DOI:10.1016/S0040-4039(01)80627-4