C₆₆H₄₂N₄

Base Information

Chemical Name:C₆₆H₄₂N₄
CAS No.:1571074-49-1
Molecular Formula:C₆₆H₄₂N₄
Molecular Weight:891.086
Hs Code.:

C<sub>66</sub>H<sub>42</sub>N<sub>4</sub>

Synonyms:C₆₆H₄₂N₄

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Chemical Property of C₆₆H₄₂N₄

Chemical Property:

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Technology Process of C₆₆H₄₂N₄

There total 5 articles about C₆₆H₄₂N₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 1571074-44-6
pseudogem-4,15-bis(2,5-diphenyl-1H-imidazol-4-yl)[2.2]paracyclophane

: 1571074-49-1
C₆₆H₄₂N₄

Guidance literature:: With potassium hydroxide; potassium hexacyanoferrate(III); In benzene; at 20 ℃; for 3h;
DOI:10.1021/ja501028v

Reference yield:

: 591-50-4
iodobenzene

: 1571074-49-1
C₆₆H₄₂N₄

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 30 h / 80 °C / Inert atmosphere

2: tetraethylammonium bromide; sodium hydrogencarbonate; potassium permanganate / dichloromethane / 52 h / 20 °C

3: ammonium acetate; acetic acid / 12 h / 110 °C

4: potassium hexacyanoferrate(III); potassium hydroxide / benzene / 3 h / 20 °C

With potassium permanganate; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetraethylammonium bromide; ammonium acetate; sodium hydrogencarbonate; acetic acid; triethylamine; potassium hydroxide; potassium hexacyanoferrate(III); In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1021/ja501028v

Reference yield:

: 823192-06-9,823192-26-3,1037412-89-7
pseudo-gem-diethynyl[2.2]paracyclophane

: 1571074-49-1
C₆₆H₄₂N₄

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 30 h / 80 °C / Inert atmosphere

2: tetraethylammonium bromide; sodium hydrogencarbonate; potassium permanganate / dichloromethane / 52 h / 20 °C

3: ammonium acetate; acetic acid / 12 h / 110 °C

4: potassium hexacyanoferrate(III); potassium hydroxide / benzene / 3 h / 20 °C

With potassium permanganate; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetraethylammonium bromide; ammonium acetate; sodium hydrogencarbonate; acetic acid; triethylamine; potassium hydroxide; potassium hexacyanoferrate(III); In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1021/ja501028v