1-{4-(bromomethyl)benzyl}-N-(1H-imidazoline-2-yl)-1H-benzimidazol-2-amine

Base Information

Chemical Name:1-{4-(bromomethyl)benzyl}-N-(1H-imidazoline-2-yl)-1H-benzimidazol-2-amine
CAS No.:1380317-23-6
Molecular Formula:C₁₈H₁₈BrN₅
Molecular Weight:384.278
Hs Code.:

Synonyms:1-{4-(bromomethyl)benzyl}-N-(1H-imidazoline-2-yl)-1H-benzimidazol-2-amine

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Chemical Property of 1-{4-(bromomethyl)benzyl}-N-(1H-imidazoline-2-yl)-1H-benzimidazol-2-amine

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Technology Process of 1-{4-(bromomethyl)benzyl}-N-(1H-imidazoline-2-yl)-1H-benzimidazol-2-amine

There total 3 articles about 1-{4-(bromomethyl)benzyl}-N-(1H-imidazoline-2-yl)-1H-benzimidazol-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 623-24-5
1,4-bis(bromomethyl)benzene

: 41926-68-5
N-(1H-benzimidazole-2-yl)-N-(4,5-dihydro-1H-imidazol-2-yl)amine

: 1380317-23-6
1-{4-(bromomethyl)benzyl}-N-(1H-imidazoline-2-yl)-1H-benzimidazol-2-amine

Guidance literature:: With sodium hydroxide; In dimethyl sulfoxide; at 35 - 40 ℃; for 2h;
DOI:10.1080/00397911.2011.567883

Reference yield:

: 934-32-7
1H-benzimidazol-2-amine

: 1380317-23-6
1-{4-(bromomethyl)benzyl}-N-(1H-imidazoline-2-yl)-1H-benzimidazol-2-amine

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 0.87 h / 125 °C / 760.05 Torr / Microwave irradiation

2: triethylamine / tetrahydrofuran / 0.17 h / Reflux; Microwave irradiation

3: sodium hydroxide / dimethyl sulfoxide / 2 h / 35 - 40 °C

With pyridine; triethylamine; sodium hydroxide; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1080/00397911.2011.567883

Reference yield:

: 884-24-2
N-(1H-imidazoline-2-yl)-1H-benzimidazol-2-amine hydroiodide

: 1380317-23-6
1-{4-(bromomethyl)benzyl}-N-(1H-imidazoline-2-yl)-1H-benzimidazol-2-amine

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 0.17 h / Reflux; Microwave irradiation

2: sodium hydroxide / dimethyl sulfoxide / 2 h / 35 - 40 °C

With triethylamine; sodium hydroxide; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1080/00397911.2011.567883