C₅₃H₆₂N₆O₁₃

Base Information

Chemical Name:C₅₃H₆₂N₆O₁₃
CAS No.:1343407-39-5
Molecular Formula:C₅₃H₆₂N₆O₁₃
Molecular Weight:991.108
Hs Code.:

C<sub>53</sub>H<sub>62</sub>N<sub>6</sub>O<sub>13</sub>

Synonyms:C₅₃H₆₂N₆O₁₃

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Chemical Property of C₅₃H₆₂N₆O₁₃

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Technology Process of C₅₃H₆₂N₆O₁₃

There total 15 articles about C₅₃H₆₂N₆O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1343407-38-4
C₅₃H₆₄N₆O₁₃

: 1343407-39-5
C₅₃H₆₂N₆O₁₃

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 6.5h;

Reference yield: 52.0%

: C₅₃H₆₄N₆O₁₃

: 1343407-39-5
C₅₃H₆₂N₆O₁₃

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 6.5h;

Reference yield:

: C₁₅H₁₈N₂O₈

: 1343407-39-5
C₅₃H₆₂N₆O₁₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: trichloroisocyanuric acid; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / 0 °C

2.1: 2,6-dimethylpyridine / dichloromethane / 1 h / -45 - 40 °C / Inert atmosphere

3.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / Inert atmosphere

4.1: lithium borohydride; ethanol / tetrahydrofuran / 1 h / 15 - 25 °C / Cooling with ice

5.1: zinc; acetic acid / ethanol / 0.08 h / Reflux

6.1: triethylamine / tetrahydrofuran / 0.17 h / 0 °C

6.2: 20 - 65 °C

7.1: potassium carbonate / water; methanol / 0.83 h / 20 °C

8.1: Dess-Martin periodane / dichloromethane / 6.5 h / 20 °C

With 2,6-dimethylpyridine; lithium borohydride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; ethanol; trichloroisocyanuric acid; sodium carbonate; potassium carbonate; Dess-Martin periodane; acetic acid; triethylamine; zinc; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene; 3.1: Suzuki Coupling;