5'-O-tert-butyldimethylsilyl-2',3'-O-isopropylidene-N³-(p-methoxybenzyl)-6-ethyluridine

Base Information

• Chemical Name: 5'-O-tert-butyldimethylsilyl-2',3'-O-isopropylidene-N³-(p-methoxybenzyl)-6-ethyluridine
• CAS No.: 1429644-30-3
• Molecular Formula: C₂₈H₄₂N₂O₇Si
• Molecular Weight: 546.736

Synonyms:5'-O-tert-butyldimethylsilyl-2',3'-O-isopropylidene-N³-(p-methoxybenzyl)-6-ethyluridine

Chemical Property of 5'-O-tert-butyldimethylsilyl-2',3'-O-isopropylidene-N³-(p-methoxybenzyl)-6-ethyluridine

Chemical Property:

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Technology Process of 5'-O-tert-butyldimethylsilyl-2',3'-O-isopropylidene-N³-(p-methoxybenzyl)-6-ethyluridine

There total 1 articles about 5'-O-tert-butyldimethylsilyl-2',3'-O-isopropylidene-N³-(p-methoxybenzyl)-6-ethyluridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

5'-O-tert-butyldimethylsilyl-2',3'-O-isopropylidene-N3-(p-methoxybenzyl)-6-cyanouridine (1429644-28-9) + ethylmagnesium bromide (925-90-6) → 5'-O-tert-butyldimethylsilyl-2',3'-O-isopropylidene-N3-(p-methoxybenzyl)-6-ethyluridine (1429644-30-3)

Guidance literature:

With zinc(II) chloride; In tetrahydrofuran; diethyl ether; at 0 - 20 ℃; for 3h;

DOI:10.1021/jo400364p

upstream raw materials:

5'-O-tert-butyldimethylsilyl-2',3'-O-isopropylidene-N³-(p-methoxybenzyl)-6-cyanouridine

ethylmagnesium bromide

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