(R)-ethyl 2-(4-((tert-butoxycarbonylamino)methyl)phenylamino)-3-methylbutanoate

Base Information

Chemical Name:(R)-ethyl 2-(4-((tert-butoxycarbonylamino)methyl)phenylamino)-3-methylbutanoate
CAS No.:1283679-35-5
Molecular Formula:C₁₉H₃₀N₂O₄
Molecular Weight:350.458
Hs Code.:

Synonyms:(R)-ethyl 2-(4-((tert-butoxycarbonylamino)methyl)phenylamino)-3-methylbutanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-ethyl 2-(4-((tert-butoxycarbonylamino)methyl)phenylamino)-3-methylbutanoate

Chemical Property:

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Technology Process of (R)-ethyl 2-(4-((tert-butoxycarbonylamino)methyl)phenylamino)-3-methylbutanoate

There total 5 articles about (R)-ethyl 2-(4-((tert-butoxycarbonylamino)methyl)phenylamino)-3-methylbutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34619-03-9
tert-butyldicarbonate

: 1041629-69-9
C₁₄H₂₂N₂O₂

: 1283679-35-5
(R)-ethyl 2-(4-((tert-butoxycarbonylamino)methyl)phenylamino)-3-methylbutanoate

Guidance literature:: With sodium hydrogencarbonate; at 20 ℃; for 3h;
DOI:10.1016/j.bmcl.2011.01.041

Reference yield:

: C₁₂H₁₄N₂O₂

: 1283679-35-5
(R)-ethyl 2-(4-((tert-butoxycarbonylamino)methyl)phenylamino)-3-methylbutanoate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetone / 2 h

2: sodium tetrahydroborate; nickel dichloride / ethanol / 0.33 h / 20 °C

3: sodium hydrogencarbonate / 3 h / 20 °C

With sodium tetrahydroborate; sodium hydrogencarbonate; potassium carbonate; nickel dichloride; In ethanol; acetone;
DOI:10.1016/j.bmcl.2011.01.041

Reference yield:

: 1283679-26-4
(R)-ethyl 2-(4-cyanophenylamino)-3-methylbutanoate

: 1283679-35-5
(R)-ethyl 2-(4-((tert-butoxycarbonylamino)methyl)phenylamino)-3-methylbutanoate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate; nickel dichloride / ethanol / 0.33 h / 20 °C

2: sodium hydrogencarbonate / 3 h / 20 °C

With sodium tetrahydroborate; sodium hydrogencarbonate; nickel dichloride; In ethanol;
DOI:10.1016/j.bmcl.2011.01.041