all-trans-1-benzyloxy-3,7,11,15,19,23-hexamethyl-9-(p-tolylsulfonyl)-2,6,10,14,18,22-tetracosahexaene

Base Information

Chemical Name:all-trans-1-benzyloxy-3,7,11,15,19,23-hexamethyl-9-(p-tolylsulfonyl)-2,6,10,14,18,22-tetracosahexaene
CAS No.:68690-53-9
Molecular Formula:C₄₄H₆₂O₃S
Molecular Weight:671.04
Hs Code.:

Synonyms:all-trans-1-benzyloxy-3,7,11,15,19,23-hexamethyl-9-(p-tolylsulfonyl)-2,6,10,14,18,22-tetracosahexaene

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Chemical Property of all-trans-1-benzyloxy-3,7,11,15,19,23-hexamethyl-9-(p-tolylsulfonyl)-2,6,10,14,18,22-tetracosahexaene

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Technology Process of all-trans-1-benzyloxy-3,7,11,15,19,23-hexamethyl-9-(p-tolylsulfonyl)-2,6,10,14,18,22-tetracosahexaene

There total 4 articles about all-trans-1-benzyloxy-3,7,11,15,19,23-hexamethyl-9-(p-tolylsulfonyl)-2,6,10,14,18,22-tetracosahexaene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.9%

: 52220-07-2
trans,trans-1-benzyloxy-8-chloro-3,7-dimethyl-2,6-octadiene

: 68690-47-1
1-methyl-4-{[(2E,6E,10E)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraen-1-yl]sulfonyl}benzene

: 68690-53-9
all-trans-1-benzyloxy-3,7,11,15,19,23-hexamethyl-9-(p-tolylsulfonyl)-2,6,10,14,18,22-tetracosahexaene

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; N,N-dimethyl-formamide; at -20 ℃; for 0.333333h;
DOI:10.1246/bcsj.54.3530

Reference yield:

: 50848-64-1
2E,6E,10E-geranylgeranyl bromide

: 68690-53-9
all-trans-1-benzyloxy-3,7,11,15,19,23-hexamethyl-9-(p-tolylsulfonyl)-2,6,10,14,18,22-tetracosahexaene

Guidance literature:: Multi-step reaction with 2 steps

1: dimethylformamide / 1 h / Ambient temperature

2: 88.9 percent / t-BuOK / tetrahydrofuran; dimethylformamide / 0.33 h / -20 °C

With potassium tert-butylate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.54.3530

Reference yield:

: 24034-73-9
Geranylgeraniol

: 68690-53-9
all-trans-1-benzyloxy-3,7,11,15,19,23-hexamethyl-9-(p-tolylsulfonyl)-2,6,10,14,18,22-tetracosahexaene

Guidance literature:: Multi-step reaction with 3 steps

1: PBr₃ / dimethylformamide / 0.25 h / -10 - -7 °C

2: dimethylformamide / 1 h / Ambient temperature

3: 88.9 percent / t-BuOK / tetrahydrofuran; dimethylformamide / 0.33 h / -20 °C

With potassium tert-butylate; phosphorus tribromide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.54.3530