ethyl α-<(diphenylmethylene)amino>-(+/-)-3-indolacetate

Base Information

Chemical Name:ethyl α-<(diphenylmethylene)amino>-(+/-)-3-indolacetate
CAS No.:120133-83-7
Molecular Formula:C₂₅H₂₂N₂O₂
Molecular Weight:382.462
Hs Code.:

Synonyms:ethyl α-<(diphenylmethylene)amino>-(+/-)-3-indolacetate

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Chemical Property of ethyl α-<(diphenylmethylene)amino>-(+/-)-3-indolacetate

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Technology Process of ethyl α-<(diphenylmethylene)amino>-(+/-)-3-indolacetate

There total 1 articles about ethyl α-<(diphenylmethylene)amino>-(+/-)-3-indolacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 120-72-9
indole

: 97611-55-7
ethyl 2-acetoxy-2-diphenylmethyleneaminoacetate

: 120133-83-7
ethyl α-<(diphenylmethylene)amino>-(+/-)-3-indolacetate

Guidance literature:: With titanium tetrachloride; In dichloromethane; at -78 ℃; for 3h;
DOI:10.1016/S0040-4020(01)86045-2

Reference yield:

: 120133-83-7
ethyl α-<(diphenylmethylene)amino>-(+/-)-3-indolacetate

: 6747-15-5
α-amino-(+/)-3-indoleacetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1 M hydrochloric acid / diethyl ether; H₂O / 4 h / Ambient temperature

2: sat. lithium hydroxide monohydrate / H₂O / 2 h / Ambient temperature

With hydrogenchloride; lithium hydroxide; In diethyl ether; water;
DOI:10.1016/S0040-4020(01)86045-2