Benzyl (6-bromohexyl)carbamate

Base Information

Chemical Name:Benzyl (6-bromohexyl)carbamate
CAS No.:116784-97-5
Molecular Formula:C14H20BrNO2
Molecular Weight:314.222
Hs Code.:2924299090
European Community (EC) Number:675-727-5
DSSTox Substance ID:DTXSID40570237
Nikkaji Number:J1.854.437G
Wikidata:Q82457622
Mol file:116784-97-5.mol

Synonyms:116784-97-5;Benzyl (6-bromohexyl)carbamate;N-Cbz-6-Bromo-hexylamine;BENZYL N-(6-BROMOHEXYL)CARBAMATE;benzyl 6-bromohexylcarbamate;Carbamic acid, N-(6-bromohexyl)-, phenylmethyl ester;(6-bromo-hexyl)-carbamic acid benzyl ester;N-(6-bromohexyl)carbamic acid (phenylmethyl) ester;Benzyl(6-bromohexyl)carbamate;SCHEMBL5240928;DTXSID40570237;MFCD08436190;AKOS015912148;(6-bromohexyl)carbamic acid benzyl ester;AS-36732;(6-Bromohexyl)-carbamic acid benzyl ester;B5355;CS-0149756;A803670;benzyl N-(6-bromohexyl)carbamate;N-CBZ-6-BROMO-HEXYLAMINE

Suppliers and Price of Benzyl (6-bromohexyl)carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
N-Cbz-6-bromo-hexylamine
100mg
$ 65.00

TCI Chemical
Benzyl (6-Bromohexyl)carbamate
200MG
$ 70.00

TCI Chemical
Benzyl (6-Bromohexyl)carbamate
1G
$ 243.00

Crysdot
Benzyl (6-Bromohexyl)carbamate 97%
5g
$ 478.00

AstaTech
N-CBZ-6-BROMO-HEXYLAMINE 97%
1 / G
$ 170.00

AstaTech
N-CBZ-6-BROMO-HEXYLAMINE 97%
5 / G
$ 510.00

AstaTech
N-CBZ-6-BROMO-HEXYLAMINE 97%
25 / G
$ 1529.00

American Custom Chemicals Corporation
N-CBZ-6-BROMO-HEXYLAMINE 95.00%
5G
$ 1334.03

American Custom Chemicals Corporation
N-CBZ-6-BROMO-HEXYLAMINE 95.00%
1G
$ 782.23

Ambeed
Benzyl (6-Bromohexyl)carbamate 97%
1g
$ 149.00

Total 21 raw suppliers

Chemical Property of Benzyl (6-bromohexyl)carbamate

Chemical Property:

Vapor Pressure:2.37E-07mmHg at 25°C
Melting Point:43-45 °C
Refractive Index:1.533
Boiling Point:422.7 °C at 760 mmHg
PKA:12.70±0.46(Predicted)
Flash Point:209.4 °C
PSA：38.33000
Density:1.273 g/cm³
LogP:4.25900
Storage Temp.:Sealed in dry,Room Temperature
Solubility.:soluble in Methanol
XLogP3:3.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:9
Exact Mass:313.06774
Heavy Atom Count:18
Complexity:218

Purity/Quality:

97% ^*data from raw suppliers

N-Cbz-6-bromo-hexylamine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)COC(=O)NCCCCCCBr

Technology Process of Benzyl (6-bromohexyl)carbamate

There total 4 articles about Benzyl (6-bromohexyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 17996-12-2
N-benzyloxycarbonyl-6-amino-1-hexanol

: 116784-97-5
N-benzyloxycarbonyl-6-bromo-1-hexylamine

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1055/s-0034-1378537

Reference yield:

: 4048-33-3
6-amino-1-hexanol

: 116784-97-5
N-benzyloxycarbonyl-6-bromo-1-hexylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / triethylamine / methanol / 10 h / 20 °C

2: 84 percent / CBr₄; PPh₃ / CH₂Cl₂ / 0 - 20 °C

With carbon tetrabromide; triethylamine; triphenylphosphine; In methanol; dichloromethane;
DOI:10.1021/ja039465q

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 116784-97-5
N-benzyloxycarbonyl-6-bromo-1-hexylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / triethylamine / methanol / 10 h / 20 °C

2: 84 percent / CBr₄; PPh₃ / CH₂Cl₂ / 0 - 20 °C

With carbon tetrabromide; triethylamine; triphenylphosphine; In methanol; dichloromethane;
DOI:10.1021/ja039465q