Acetic acid (E)-(R)-8-(4-methoxy-benzyloxy)-3,7-dimethyl-oct-6-enyl ester

Base Information

Chemical Name:Acetic acid (E)-(R)-8-(4-methoxy-benzyloxy)-3,7-dimethyl-oct-6-enyl ester
CAS No.:149710-28-1
Molecular Formula:C₂₀H₃₀O₄
Molecular Weight:334.456
Hs Code.:

Synonyms:Acetic acid (E)-(R)-8-(4-methoxy-benzyloxy)-3,7-dimethyl-oct-6-enyl ester

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Chemical Property of Acetic acid (E)-(R)-8-(4-methoxy-benzyloxy)-3,7-dimethyl-oct-6-enyl ester

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Technology Process of Acetic acid (E)-(R)-8-(4-methoxy-benzyloxy)-3,7-dimethyl-oct-6-enyl ester

There total 4 articles about Acetic acid (E)-(R)-8-(4-methoxy-benzyloxy)-3,7-dimethyl-oct-6-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 824-94-2
p-methoxybenzyl chloride

: 149818-99-5
(6R)-8-acetoxy-2,6-dimethyl-2-octen-1-ol

: 149710-28-1
Acetic acid (E)-(R)-8-(4-methoxy-benzyloxy)-3,7-dimethyl-oct-6-enyl ester

Guidance literature:: With silver(l) oxide; In diethyl ether; for 4h; Heating;
DOI:10.1021/jo00068a021

Reference yield:

: 1117-61-9
(3R)-citronellol

: 149710-28-1
Acetic acid (E)-(R)-8-(4-methoxy-benzyloxy)-3,7-dimethyl-oct-6-enyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / pyridine / CH₂Cl₂ / Ambient temperature

2: 42 percent / SeO₂, t-BuOOH, salicylic acid / CH₂Cl₂ / 42 h / Ambient temperature

3: 49 percent / Ag₂O / diethyl ether / 4 h / Heating

With pyridine; tert.-butylhydroperoxide; selenium(IV) oxide; salicylic acid; silver(l) oxide; In diethyl ether; dichloromethane;
DOI:10.1021/jo00068a021

Reference yield:

: 20425-54-1,67650-82-2
(R)-1-citronellyl acetate

: 149710-28-1
Acetic acid (E)-(R)-8-(4-methoxy-benzyloxy)-3,7-dimethyl-oct-6-enyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 42 percent / SeO₂, t-BuOOH, salicylic acid / CH₂Cl₂ / 42 h / Ambient temperature

2: 49 percent / Ag₂O / diethyl ether / 4 h / Heating

With tert.-butylhydroperoxide; selenium(IV) oxide; salicylic acid; silver(l) oxide; In diethyl ether; dichloromethane;
DOI:10.1021/jo00068a021