Technology Process of C23H23NO3
There total 2 articles about C23H23NO3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
3-(1-oxopropyl)-4-(diphenylmethyl)-2-oxazolidinone;
With
sodium hexamethyldisilazane;
In
tetrahydrofuran;
at -78 ℃;
Inert atmosphere;
propargyl iodide;
In
tetrahydrofuran;
at -78 ℃;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran; hexanes / -78 °C / Inert atmosphere
1.2: -78 °C
2.1: sodium hexamethyldisilazane / tetrahydrofuran / -78 °C / Inert atmosphere
2.2: -78 °C
With
n-butyllithium; sodium hexamethyldisilazane;
In
tetrahydrofuran; hexanes;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: water; lithium hydroxide / tetrahydrofuran / 20 °C
1.2: pH 3 - 4
2.1: 4-methyl-morpholine; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine / tetrahydrofuran / 20 °C
2.2: 20 °C
3.1: n-butyllithium / tetrahydrofuran; hexanes / 1 h / 78 °C / Inert atmosphere
3.2: -78 °C
4.1: sodium hydride / tetrahydrofuran / 0 - 10 °C / Inert atmosphere
4.2: 20 °C
5.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 0 - 10 °C
6.1: hydrogenchloride; water / methanol / 20 °C
7.1: sodium hydroxide; water / methanol / 20 - 55 °C
7.2: pH 2 - 3
8.1: sodium hydroxide / water; methanol / 20 °C
With
4-methyl-morpholine; hydrogenchloride; sodium tetrahydroborate; n-butyllithium; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine; cerium(III) chloride heptahydrate; water; sodium hydride; sodium hydroxide; lithium hydroxide;
In
tetrahydrofuran; methanol; hexanes; water;
