2-bromo-N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-(phenylmethyl)acetamide

Base Information

Chemical Name:2-bromo-N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-(phenylmethyl)acetamide
CAS No.:82082-41-5
Molecular Formula:C₂₂H₁₅BrCl₃NO₂
Molecular Weight:511.63
Hs Code.:

Synonyms:2-bromo-N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-(phenylmethyl)acetamide

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Chemical Property of 2-bromo-N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-(phenylmethyl)acetamide

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Technology Process of 2-bromo-N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-(phenylmethyl)acetamide

There total 8 articles about 2-bromo-N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-(phenylmethyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 82082-32-4
<5-chloro-2-<(phenylmethyl)amino>phenyl>(2,6-dichlorophenyl)methanone

: 598-21-0
2-Bromoacetyl bromide

: 82082-41-5
2-bromo-N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-(phenylmethyl)acetamide

Guidance literature:: With pyridine; In diethyl ether; for 0.333333h; Ambient temperature;
DOI:10.1021/jm00351a009

Reference yield:

: 6628-86-0
5-chloro-2-nitrobenzaldehyde

: 82082-41-5
2-bromo-N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-(phenylmethyl)acetamide

Guidance literature:: Multi-step reaction with 7 steps

1: 1.) n-BuLi / 1.) THF, -78 deg C, 20 min, 2.) THF, -78 deg C, 1 h

2: Jones reagent, acetic acid / diethyl ether / 12 h / Ambient temperature

3: 62 percent / H₂ / Raney nickel / ethanol / 8 h / 760 Torr

4: 84 percent / pyridine / diethyl ether; CH₂Cl₂ / 1 h / Ambient temperature

5: 1.) n-BuLi / 1.) hexane, DMSO, 2.) hexane, DMSO, RT, 1 h

6: 70 percent / NaOH / aq. ethanol / 72 h / Heating

7: 100 percent / pyridine / diethyl ether / 0.33 h / Ambient temperature

With pyridine; sodium hydroxide; n-butyllithium; jones reagent; hydrogen; acetic acid; nickel; In diethyl ether; ethanol; dichloromethane;
DOI:10.1021/jm00351a009

Reference yield:

: 82082-25-5
(2,6-dichlorophenyl)(5-chloro-2-nitrophenyl)methanone

: 82082-41-5
2-bromo-N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-(phenylmethyl)acetamide

Guidance literature:: Multi-step reaction with 5 steps

1: 62 percent / H₂ / Raney nickel / ethanol / 8 h / 760 Torr

2: 84 percent / pyridine / diethyl ether; CH₂Cl₂ / 1 h / Ambient temperature

3: 1.) n-BuLi / 1.) hexane, DMSO, 2.) hexane, DMSO, RT, 1 h

4: 70 percent / NaOH / aq. ethanol / 72 h / Heating

5: 100 percent / pyridine / diethyl ether / 0.33 h / Ambient temperature

With pyridine; sodium hydroxide; n-butyllithium; hydrogen; nickel; In diethyl ether; ethanol; dichloromethane;
DOI:10.1021/jm00351a009