5-allyloxy-2-hydroxybenzoic acid

Base Information

• Chemical Name: 5-allyloxy-2-hydroxybenzoic acid
• CAS No.: 84213-04-7
• Molecular Formula: C₁₀H₁₀O₄
• Molecular Weight: 194.187
• Mol file: 84213-04-7.mol

Synonyms:5-allyloxy-2-hydroxybenzoic acid

Chemical Property of 5-allyloxy-2-hydroxybenzoic acid

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 5-allyloxy-2-hydroxybenzoic acid

There total 2 articles about 5-allyloxy-2-hydroxybenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.9%

2,5-dihydroxybenzoic acid. (490-79-9) + allyl bromide (106-95-6) → 5-allyloxy-2-hydroxybenzoic acid (84213-04-7)

Guidance literature:

2,5-dihydroxybenzoic acid.; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 2h;

allyl bromide; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 2h;

Reference yield:

→ 5-allyloxy-2-hydroxybenzoic acid (84213-04-7)

Guidance literature:

2-Hydroxy-5-allyloxy-benzoesaeure-methylester, wss.-methanol. NaOH;

Reference yield: 79.0%

5-allyloxy-2-hydroxybenzoic acid (84213-04-7) → 5-allyloxy-2-hydroxytoluene (79950-48-4)

Guidance literature:

5-allyloxy-2-hydroxybenzoic acid; With chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 3h;

With sodium tetrahydroborate; In tetrahydrofuran; water; at 0 - 20 ℃;

With hydrogenchloride; In tetrahydrofuran; water; pH=6;

upstream raw materials:

2,5-dihydroxybenzoic acid.

allyl bromide

Downstream raw materials:

5-allyloxy-2-hydroxytoluene