Technology Process of C57H60N12O24
There total 4 articles about C57H60N12O24 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(II) sulfate; sodium L-ascorbate;
In
water; N,N-dimethyl-formamide;
at 120 ℃;
for 0.333333h;
Microwave irradiation;
DOI:10.1021/ol4004367
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 3.5 h / 20 °C / Darkness
2: caesium carbonate / N,N-dimethyl-formamide / 1.5 h / 20 °C / Darkness
3: sulfuric acid / dichloromethane; methanol / 2 h / 20 °C / Darkness
4: copper(II) sulfate; sodium L-ascorbate / N,N-dimethyl-formamide; water / 0.33 h / 120 °C / Microwave irradiation
With
dmap; sulfuric acid; caesium carbonate; copper(II) sulfate; sodium L-ascorbate; dicyclohexyl-carbodiimide;
In
methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ol4004367
- Guidance literature:
-
Multi-step reaction with 3 steps
1: caesium carbonate / N,N-dimethyl-formamide / 1.5 h / 20 °C / Darkness
2: sulfuric acid / dichloromethane; methanol / 2 h / 20 °C / Darkness
3: copper(II) sulfate; sodium L-ascorbate / N,N-dimethyl-formamide; water / 0.33 h / 120 °C / Microwave irradiation
With
sulfuric acid; caesium carbonate; copper(II) sulfate; sodium L-ascorbate;
In
methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ol4004367