Technology Process of C29H34N4O3S
There total 5 articles about C29H34N4O3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
p-methoxybenzylmercaptan;
With
sodium hydride;
In
N,N-dimethyl-formamide;
at 25 ℃;
for 0.5h;
Inert atmosphere;
C21H25BrN4O2;
In
N,N-dimethyl-formamide;
at 25 ℃;
for 10h;
Inert atmosphere;
DOI:10.1039/c3cc37265k
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sulfuric acid / water / 1.5 h / 115 - 125 °C / Inert atmosphere
2.1: pyridine; 1,8-diazabicyclo[5.4.0]undec-7-ene / 36 h / Reflux; Inert atmosphere
3.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 8 h / 70 °C / Inert atmosphere
4.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 25 °C / Inert atmosphere
4.2: 10 h / 25 °C / Inert atmosphere
With
pyridine; N-Bromosuccinimide; sulfuric acid; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; dibenzoyl peroxide;
In
tetrachloromethane; water; N,N-dimethyl-formamide;
DOI:10.1039/c3cc37265k
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: pyridine; 1,8-diazabicyclo[5.4.0]undec-7-ene / 36 h / Reflux; Inert atmosphere
2.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 8 h / 70 °C / Inert atmosphere
3.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 25 °C / Inert atmosphere
3.2: 10 h / 25 °C / Inert atmosphere
With
pyridine; N-Bromosuccinimide; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; dibenzoyl peroxide;
In
tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c3cc37265k
