Thiocarbonic acid O-p-tolyl ester O-((3aR,5aR,8aR)-3a,5,5-trimethyl-8-oxo-decahydro-cyclopenta[c]pentalen-1-yl) ester

Base Information

Chemical Name:Thiocarbonic acid O-p-tolyl ester O-((3aR,5aR,8aR)-3a,5,5-trimethyl-8-oxo-decahydro-cyclopenta[c]pentalen-1-yl) ester
CAS No.:87802-45-7
Molecular Formula:C₂₂H₂₈O₃S
Molecular Weight:372.529
Hs Code.:

Synonyms:Thiocarbonic acid O-p-tolyl ester O-((3aR,5aR,8aR)-3a,5,5-trimethyl-8-oxo-decahydro-cyclopenta[c]pentalen-1-yl) ester

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Chemical Property of Thiocarbonic acid O-p-tolyl ester O-((3aR,5aR,8aR)-3a,5,5-trimethyl-8-oxo-decahydro-cyclopenta[c]pentalen-1-yl) ester

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Technology Process of Thiocarbonic acid O-p-tolyl ester O-((3aR,5aR,8aR)-3a,5,5-trimethyl-8-oxo-decahydro-cyclopenta[c]pentalen-1-yl) ester

There total 3 articles about Thiocarbonic acid O-p-tolyl ester O-((3aR,5aR,8aR)-3a,5,5-trimethyl-8-oxo-decahydro-cyclopenta[c]pentalen-1-yl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 937-63-3
p-Tolyl chlorothionoformate

: 82995-43-5,86161-33-3,86161-34-4
7-hydroxy-2,2,4-trimethyltricyclo<6.3.0.0^4,8>undecan-9-one

: 87802-45-7
Thiocarbonic acid O-p-tolyl ester O-((3aR,5aR,8aR)-3a,5,5-trimethyl-8-oxo-decahydro-cyclopenta[c]pentalen-1-yl) ester

Guidance literature:: With pyridine; In tetrahydrofuran;
DOI:10.1021/jo00142a037

Reference yield:

: (3aS,6R,6aR)-6-(2-[1,3]Dioxan-2-yl-ethyl)-4,4,6-trimethyl-hexahydro-pentalen-1-one

: 87802-45-7
Thiocarbonic acid O-p-tolyl ester O-((3aR,5aR,8aR)-3a,5,5-trimethyl-8-oxo-decahydro-cyclopenta[c]pentalen-1-yl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: HCl / H₂O; tetrahydrofuran

2: 84 percent / pyridine / tetrahydrofuran / Ambient temperature

With pyridine; hydrogenchloride; In tetrahydrofuran; water;
DOI:10.1021/ja00363a024

Reference yield:

: 82995-42-4
2,4,4-trimethylbicyclo<3.3.0>oct-1-en-8-one

: 87802-45-7
Thiocarbonic acid O-p-tolyl ester O-((3aR,5aR,8aR)-3a,5,5-trimethyl-8-oxo-decahydro-cyclopenta[c]pentalen-1-yl) ester

Guidance literature:: Multi-step reaction with 3 steps

1: CuBr*Me₂S

2: HCl / H₂O; tetrahydrofuran

3: 84 percent / pyridine / tetrahydrofuran / Ambient temperature

With pyridine; hydrogenchloride; copper(I) bromide dimethylsulfide complex; In tetrahydrofuran; water;
DOI:10.1021/ja00363a024