diethyl (S)-hydroxy[(2R)-5-oxo-2,5-dihydrofuran-2-yl]phenylmethylphosphonate

Base Information

Chemical Name:diethyl (S)-hydroxy[(2R)-5-oxo-2,5-dihydrofuran-2-yl]phenylmethylphosphonate
CAS No.:1602489-92-8
Molecular Formula:C₁₅H₁₉O₆P
Molecular Weight:326.286
Hs Code.:

Synonyms:diethyl (S)-hydroxy[(2R)-5-oxo-2,5-dihydrofuran-2-yl]phenylmethylphosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl (S)-hydroxy[(2R)-5-oxo-2,5-dihydrofuran-2-yl]phenylmethylphosphonate

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Technology Process of diethyl (S)-hydroxy[(2R)-5-oxo-2,5-dihydrofuran-2-yl]phenylmethylphosphonate

There total 3 articles about diethyl (S)-hydroxy[(2R)-5-oxo-2,5-dihydrofuran-2-yl]phenylmethylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 61550-02-5
(furan-2-yloxy)-trimethylsilane

: 3277-27-8
diethyl benzoylphosphonate

: 1602489-92-8
diethyl (S)-hydroxy[(2R)-5-oxo-2,5-dihydrofuran-2-yl]phenylmethylphosphonate

Guidance literature:: With 2,2,2-trifluoroethanol; copper(II) bis(trifluoromethanesulfonate); (S)-N-[2-(2,4,6-triisopropylbenzylamino)phenyl]-S-methyl-S-phenylsulfoximine; In diethyl ether; at 0 ℃; Reagent/catalyst; Solvent; Temperature; stereoselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1002/chem.201304331

Reference yield:

: 61550-02-5
(furan-2-yloxy)-trimethylsilane

: 3277-27-8
diethyl benzoylphosphonate

: 1602489-92-8
diethyl (S)-hydroxy[(2R)-5-oxo-2,5-dihydrofuran-2-yl]phenylmethylphosphonate

: diethyl (R)-hydroxy[(2S)-5-oxo-2,5-dihydrofuran-2-yl]phenylmethylphosphonate

Guidance literature:: With copper(II) bis(trifluoromethanesulfonate); (S)-N-[2-(2,4,6-triisopropylbenzylamino)phenyl]-S-methyl-S-phenylsulfoximine; In dichloromethane; at 20 ℃; Reagent/catalyst; Solvent; Overall yield = 91 %; stereoselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1002/chem.201304331

Reference yield:

: 61550-02-5
(furan-2-yloxy)-trimethylsilane

: 3277-27-8
diethyl benzoylphosphonate

: 1602489-92-8
diethyl (S)-hydroxy[(2R)-5-oxo-2,5-dihydrofuran-2-yl]phenylmethylphosphonate

: diethyl (R)-hydroxy[(2S)-5-oxo-2,5-dihydrofuran-2-yl]phenylmethylphosphonate

: 1337951-99-1
diethyl hydroxy[5-oxo-2,5-dihydrofuran-2-yl]phenylmethylphosphonate

Guidance literature:: With copper(II) bis(trifluoromethanesulfonate); isopropyl alcohol; (S)-N-[2-(2,4,6-triisopropylbenzylamino)phenyl]-S-methyl-S-phenylsulfoximine; In 1,4-dioxane; at 20 ℃; Reagent/catalyst; Solvent; Overall yield = 80 %; stereoselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1002/chem.201304331