C₃₂H₃₀O₇

Base Information

• Chemical Name: C₃₂H₃₀O₇
• CAS No.: 1447605-61-9
• Molecular Formula: C₃₂H₃₀O₇
• Molecular Weight: 526.586
• Mol file: 1447605-61-9.mol

Synonyms:C₃₂H₃₀O₇

Chemical Property of C₃₂H₃₀O₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₂H₃₀O₇

There total 6 articles about C₃₂H₃₀O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-methoxy-4-(phenylmethoxy)benzaldehyde (2426-87-1) + 4-benzyloxy-6-hydroxy-2-(methoxymethoxy)acetophenone (1365537-25-2) → C32H30O7 (1447605-61-9)

Guidance literature:

4-benzyloxy-6-hydroxy-2-(methoxymethoxy)acetophenone; With sodium hydride; In n-heptane; N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.5h; Inert atmosphere;

3-methoxy-4-(phenylmethoxy)benzaldehyde; In n-heptane; N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 2.16667h; Inert atmosphere;

DOI:10.1016/j.tetasy.2013.02.012

Reference yield:

2,4,6-trihydroxyacetophenone (480-66-0,67471-34-5) → C32H30O7 (1447605-61-9)

Guidance literature:

Multi-step reaction with 5 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

1.2: 4 h / Inert atmosphere; Reflux

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 3 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 1 h / 3 °C / Inert atmosphere

4.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 75 °C / Inert atmosphere

5.1: sodium hydride / n-heptane; N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere

5.2: 2.17 h / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; tetrabutyl ammonium fluoride; sodium hydride; potassium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; n-heptane; dichloromethane; N,N-dimethyl-formamide; mineral oil; 5.1: |Aldol Condensation / 5.2: |Aldol Condensation;

DOI:10.1016/j.tetasy.2013.02.012

Reference yield:

1-{4-[(tert-butyldimethylsilyl)oxy]-2,6-dihydroxyphenyl}ethan-1-one (139140-13-9) → C32H30O7 (1447605-61-9)

Guidance literature:

Multi-step reaction with 4 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 3 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 1 h / 3 °C / Inert atmosphere

3.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 75 °C / Inert atmosphere

4.1: sodium hydride / n-heptane; N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere

4.2: 2.17 h / 0 - 20 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; sodium hydride; potassium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; n-heptane; dichloromethane; N,N-dimethyl-formamide; mineral oil; 4.1: |Aldol Condensation / 4.2: |Aldol Condensation;

DOI:10.1016/j.tetasy.2013.02.012

upstream raw materials:

3-methoxy-4-(phenylmethoxy)benzaldehyde

4-benzyloxy-6-hydroxy-2-(methoxymethoxy)acetophenone

1-{4-[(tert-butyldimethylsilyl)oxy]-2,6-dihydroxyphenyl}ethan-1-one

4-(t-butyldimethylsilyloxy)-6-hydroxy-2-(methoxymethoxy)acetophenone

Downstream raw materials:

C₃₂H₃₂O₇