C₂₃H₃₇FO₃Si

Base Information

• Chemical Name: C₂₃H₃₇FO₃Si
• CAS No.: 1402588-00-4
• Molecular Formula: C₂₃H₃₇FO₃Si
• Molecular Weight: 408.629
• Mol file: 1402588-00-4.mol

Synonyms:C₂₃H₃₇FO₃Si

Chemical Property of C₂₃H₃₇FO₃Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₂₃H₃₇FO₃Si

There total 3 articles about C₂₃H₃₇FO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C26H45FO3Si2 → C23H37FO3Si (1402588-00-4)

Guidance literature:

With sodium hydrogencarbonate; In methanol; at 25 ℃;

DOI:10.1021/bc300266y

Reference yield:

4-fluorobenzaldehyde (459-57-4) → C23H37FO3Si (1402588-00-4)

Guidance literature:

Multi-step reaction with 4 steps

1: tetrahydrofuran / 1 h / 0 °C

2: sodium hydride / N,N-dimethyl-formamide / 15 h / 22 °C

3: methyl vinyl ketone; sec.-butyllithium; copper(l) iodide / 1.5 h / -78 °C

4: sodium hydrogencarbonate / methanol / 25 °C

With copper(l) iodide; sec.-butyllithium; sodium hydride; sodium hydrogencarbonate; methyl vinyl ketone; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; 1: |Grignard Reaction / 2: |Williamson Ether Synthesis;

DOI:10.1021/bc300266y

Reference yield:

C19H31FO2Si (1402587-96-5) → C23H37FO3Si (1402588-00-4)

Guidance literature:

Multi-step reaction with 2 steps

1: methyl vinyl ketone; sec.-butyllithium; copper(l) iodide / 1.5 h / -78 °C

2: sodium hydrogencarbonate / methanol / 25 °C

With copper(l) iodide; sec.-butyllithium; sodium hydrogencarbonate; methyl vinyl ketone; In methanol;

DOI:10.1021/bc300266y

upstream raw materials:

C₁₉H₃₁FO₂Si

4-fluorobenzaldehyde

Downstream raw materials:

C₂₃H₄₀FNO₂Si