octyl 2,4,6-tri-O-benzyl-3-C-allyl-β-D-galactopyranosyl-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Base Information

Chemical Name:octyl 2,4,6-tri-O-benzyl-3-C-allyl-β-D-galactopyranosyl-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside
CAS No.:259544-03-1
Molecular Formula:C₆₅H₇₈O₁₁
Molecular Weight:1035.33
Hs Code.:

Synonyms:octyl 2,4,6-tri-O-benzyl-3-C-allyl-β-D-galactopyranosyl-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Chemical Property of octyl 2,4,6-tri-O-benzyl-3-C-allyl-β-D-galactopyranosyl-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Technology Process of octyl 2,4,6-tri-O-benzyl-3-C-allyl-β-D-galactopyranosyl-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

There total 3 articles about octyl 2,4,6-tri-O-benzyl-3-C-allyl-β-D-galactopyranosyl-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 259544-01-9
octyl 2,4,6-tri-O-benzyl-β-D-xylo-hex-3-ulopyranosyl-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 1730-25-2
allylmagnesium bromide

: 259544-03-1
octyl 2,4,6-tri-O-benzyl-3-C-allyl-β-D-galactopyranosyl-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 259544-04-2
octyl 2,4,6-tri-O-benzyl-3-C-allyl-β-D-gulopyranosyl-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: In tetrahydrofuran; diethyl ether; at 0 ℃; for 4h;
DOI:10.1021/ja993004g

Reference yield:

: 259543-99-2
octyl 3-O-allyl-2,4,6-tri-O-benzyl-β-D-galactopyranosyl-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 259544-03-1
octyl 2,4,6-tri-O-benzyl-3-C-allyl-β-D-galactopyranosyl-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / PdCl₂ / methanol / 4 h / 20 °C

2: 72 percent / Dess-Martin periodinane / CH₂Cl₂ / 1.5 h

3: 39 percent / tetrahydrofuran; diethyl ether / 4 h / 0 °C

With Dess-Martin periodane; palladium dichloride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; 1: deallylation / 2: Oxidation / 3: Addition;
DOI:10.1021/ja993004g

Reference yield:

: 259544-00-8
octyl 2,4,6-tri-O-benzyl-β-D-galactopyranosyl-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 259544-03-1
octyl 2,4,6-tri-O-benzyl-3-C-allyl-β-D-galactopyranosyl-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / Dess-Martin periodinane / CH₂Cl₂ / 1.5 h

2: 39 percent / tetrahydrofuran; diethyl ether / 4 h / 0 °C

With Dess-Martin periodane; In tetrahydrofuran; diethyl ether; dichloromethane; 1: Oxidation / 2: Addition;
DOI:10.1021/ja993004g