4-(7-(2,4-dimethoxybenzyl)-8-methyl-5,6,7,8-tetrahydro-[1,2,4]triazolo[4,3-a]pyrazin-3-yl)-2-ethylthiazole

Base Information

Chemical Name:4-(7-(2,4-dimethoxybenzyl)-8-methyl-5,6,7,8-tetrahydro-[1,2,4]triazolo[4,3-a]pyrazin-3-yl)-2-ethylthiazole
CAS No.:1429560-01-9
Molecular Formula:C₂₀H₂₅N₅O₂S
Molecular Weight:399.517
Hs Code.:

Synonyms:4-(7-(2,4-dimethoxybenzyl)-8-methyl-5,6,7,8-tetrahydro-[1,2,4]triazolo[4,3-a]pyrazin-3-yl)-2-ethylthiazole

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Chemical Property of 4-(7-(2,4-dimethoxybenzyl)-8-methyl-5,6,7,8-tetrahydro-[1,2,4]triazolo[4,3-a]pyrazin-3-yl)-2-ethylthiazole

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Technology Process of 4-(7-(2,4-dimethoxybenzyl)-8-methyl-5,6,7,8-tetrahydro-[1,2,4]triazolo[4,3-a]pyrazin-3-yl)-2-ethylthiazole

There total 4 articles about 4-(7-(2,4-dimethoxybenzyl)-8-methyl-5,6,7,8-tetrahydro-[1,2,4]triazolo[4,3-a]pyrazin-3-yl)-2-ethylthiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1429559-14-7
1-( 2,4-dimethoxybenzyl)-5-ethoxy-6-methyl-1,2,3,6-tetrahydropyrazine

: 69542-79-6
2-ethylthiazole-4-carbohydrazide

: 1429560-01-9
4-(7-(2,4-dimethoxybenzyl)-8-methyl-5,6,7,8-tetrahydro-[1,2,4]triazolo[4,3-a]pyrazin-3-yl)-2-ethylthiazole

Guidance literature:: In ethanol; at 135 ℃;

Reference yield:

: 1429559-16-9
4-(2,4-dimethoxybenzyl)-3-methylpiperazin-2-one

: 1429560-01-9
4-(7-(2,4-dimethoxybenzyl)-8-methyl-5,6,7,8-tetrahydro-[1,2,4]triazolo[4,3-a]pyrazin-3-yl)-2-ethylthiazole

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate / dichloromethane / 1 h / 20 °C / Inert atmosphere

2: ethanol / 135 °C

With sodium carbonate; In ethanol; dichloromethane;

Reference yield:

: 613-45-6
2,4-Dimethoxybenzaldehyde

: 1429560-01-9
4-(7-(2,4-dimethoxybenzyl)-8-methyl-5,6,7,8-tetrahydro-[1,2,4]triazolo[4,3-a]pyrazin-3-yl)-2-ethylthiazole

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tris(acetoxy)borohydride; acetic acid / acetonitrile / 20 °C / Inert atmosphere

2: sodium carbonate / dichloromethane / 1 h / 20 °C / Inert atmosphere

3: ethanol / 135 °C

With sodium tris(acetoxy)borohydride; sodium carbonate; acetic acid; In ethanol; dichloromethane; acetonitrile;