C₂₉H₂₈Cl₄O₅

Base Information

Chemical Name:C₂₉H₂₈Cl₄O₅
CAS No.:936338-12-4
Molecular Formula:C₂₉H₂₈Cl₄O₅
Molecular Weight:598.35
Hs Code.:

C<sub>29</sub>H<sub>28</sub>Cl<sub>4</sub>O<sub>5</sub>

Synonyms:C₂₉H₂₈Cl₄O₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₂₈Cl₄O₅

Chemical Property:

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Technology Process of C₂₉H₂₈Cl₄O₅

There total 15 articles about C₂₉H₂₈Cl₄O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 936338-11-3
C₃₀H₂₇F₃Cl₄O₈S

: 936338-12-4
C₂₉H₂₈Cl₄O₅

Guidance literature:: With formic acid; tributyl-amine; triphenylphosphine; palladium diacetate; In N,N-dimethyl-formamide; at 40 ℃; for 2h;
DOI:10.1021/jo0700474

Reference yield:

: 1025800-11-6
C₂₆H₂₈Cl₄O₄

: 936338-12-4
C₂₉H₂₈Cl₄O₅

Guidance literature:: Multi-step reaction with 12 steps

1.1: 3.50 g / lead(IV) acetate / CH₂Cl₂ / 20 °C

2.1: 53 percent / (-)-N-(1-phenylethyl)-1-azabicyclo[2.2.2]octan-3-amine; lithium chloride; n-butyllithium / tetrahydrofuran; hexane / 0.17 h / -78 °C

3.1: m-chloroperoxybenzoic acid / CH₂Cl₂ / 4 h / 20 °C

4.1: florisil / CH₂Cl₂ / 2 h

5.1: 4.90 g / IBX / dimethylsulfoxide / 1 h / 20 °C

6.1: 4.36 g / N,N-dimethylaniline / CH₂Cl₂ / -78 - 20 °C

7.1: 73 percent / tributyltin hydride; BEt₃; air / toluene; hexane / 0.5 h / 20 °C

8.1: N,N-diisopropylethylamine / CH₂Cl₂ / 4 h / -20 °C

9.1: CH₂Cl₂ / 3 h / 35 °C

9.2: 356 mg / 3-chloroperoxybenzoic acid / CH₂Cl₂ / 1 h / 20 °C

10.1: 78 percent / 3-chloroperoxybenzoic acid; BF₃*OEt₂ / CH₂Cl₂ / 0.17 h / 20 °C

11.1: 73 percent / L-selectride / tetrahydrofuran / 0.25 h / -78 °C

12.1: 92 percent / tributylamine; triphenylphosphine; formic acid / palladium(II) acetate / dimethylformamide / 2 h / 40 °C

With lead(IV) acetate; florisil; n-butyllithium; formic acid; air; tributyl-amine; triethyl borane; boron trifluoride diethyl etherate; tri-n-butyl-tin hydride; L-Selectride; N,N-dimethyl-aniline; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; lithium chloride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; palladium diacetate; In tetrahydrofuran; hexane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo0700474

Reference yield:

: C₂₆H₂₆Cl₄O₄

: 936338-12-4
C₂₉H₂₈Cl₄O₅

Guidance literature:: Multi-step reaction with 11 steps

1.1: 53 percent / (-)-N-(1-phenylethyl)-1-azabicyclo[2.2.2]octan-3-amine; lithium chloride; n-butyllithium / tetrahydrofuran; hexane / 0.17 h / -78 °C

2.1: m-chloroperoxybenzoic acid / CH₂Cl₂ / 4 h / 20 °C

3.1: florisil / CH₂Cl₂ / 2 h

4.1: 4.90 g / IBX / dimethylsulfoxide / 1 h / 20 °C

5.1: 4.36 g / N,N-dimethylaniline / CH₂Cl₂ / -78 - 20 °C

6.1: 73 percent / tributyltin hydride; BEt₃; air / toluene; hexane / 0.5 h / 20 °C

7.1: N,N-diisopropylethylamine / CH₂Cl₂ / 4 h / -20 °C

8.1: CH₂Cl₂ / 3 h / 35 °C

8.2: 356 mg / 3-chloroperoxybenzoic acid / CH₂Cl₂ / 1 h / 20 °C

9.1: 78 percent / 3-chloroperoxybenzoic acid; BF₃*OEt₂ / CH₂Cl₂ / 0.17 h / 20 °C

10.1: 73 percent / L-selectride / tetrahydrofuran / 0.25 h / -78 °C

11.1: 92 percent / tributylamine; triphenylphosphine; formic acid / palladium(II) acetate / dimethylformamide / 2 h / 40 °C

With florisil; n-butyllithium; formic acid; air; tributyl-amine; triethyl borane; boron trifluoride diethyl etherate; tri-n-butyl-tin hydride; L-Selectride; N,N-dimethyl-aniline; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; lithium chloride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; palladium diacetate; In tetrahydrofuran; hexane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo0700474