8-(2-dibenzylaminoethoxy)-1,4-dihydro-1-ethyl-4-oxo-quinoline-3-carboxylic acid hydrochloride salt

Base Information

Chemical Name:8-(2-dibenzylaminoethoxy)-1,4-dihydro-1-ethyl-4-oxo-quinoline-3-carboxylic acid hydrochloride salt
CAS No.:797052-53-0
Molecular Formula:C₂₈H₂₈N₂O₄*ClH
Molecular Weight:493.002
Hs Code.:

Synonyms:8-(2-dibenzylaminoethoxy)-1,4-dihydro-1-ethyl-4-oxo-quinoline-3-carboxylic acid hydrochloride salt

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Chemical Property of 8-(2-dibenzylaminoethoxy)-1,4-dihydro-1-ethyl-4-oxo-quinoline-3-carboxylic acid hydrochloride salt

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Technology Process of 8-(2-dibenzylaminoethoxy)-1,4-dihydro-1-ethyl-4-oxo-quinoline-3-carboxylic acid hydrochloride salt

There total 5 articles about 8-(2-dibenzylaminoethoxy)-1,4-dihydro-1-ethyl-4-oxo-quinoline-3-carboxylic acid hydrochloride salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 797052-52-9
8-(2-dibenzylaminoethoxy)-1-ethyl-4-oxo-1,4-dihydro-quinoline-3-carboxylic acid ethyl ester

: 797052-53-0
8-(2-dibenzylaminoethoxy)-1,4-dihydro-1-ethyl-4-oxo-quinoline-3-carboxylic acid hydrochloride salt

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; water; at 20 - 80 ℃; for 14.5h;

Reference yield:

: 26774-09-4,797052-49-4
8-benzyloxy-4-oxo-1,4-dihydro-quinoline-3-carboxylic acid

: 797052-53-0
8-(2-dibenzylaminoethoxy)-1,4-dihydro-1-ethyl-4-oxo-quinoline-3-carboxylic acid hydrochloride salt

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / DMF (N,N-dimethyl-formamide) / 16 h / 40 °C

2: hydrogen / palladium 10% on activated carbon / methanol / 14 h / 20 °C / 760.05 Torr

3: potassium carbonate / DMF (N,N-dimethyl-formamide) / 14 h / 70 °C

4: sodium hydroxide / tetrahydrofuran; water / 14.5 h / 20 - 80 °C

With sodium hydroxide; hydrogen; potassium carbonate; palladium 10% on activated carbon; In tetrahydrofuran; methanol; DMF (N,N-dimethyl-formamide); water;

Reference yield:

: 797052-50-7
8-benzyloxy-1-ethyl-4-oxo-1,4-dihydro-quinoline-3-carboxylic acid ethyl ester

: 797052-53-0
8-(2-dibenzylaminoethoxy)-1,4-dihydro-1-ethyl-4-oxo-quinoline-3-carboxylic acid hydrochloride salt

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / palladium 10% on activated carbon / methanol / 14 h / 20 °C / 760.05 Torr

2: potassium carbonate / DMF (N,N-dimethyl-formamide) / 14 h / 70 °C

3: sodium hydroxide / tetrahydrofuran; water / 14.5 h / 20 - 80 °C

With sodium hydroxide; hydrogen; potassium carbonate; palladium 10% on activated carbon; In tetrahydrofuran; methanol; DMF (N,N-dimethyl-formamide); water;