8-<3-propyl>-1-(4-chlorophenyl)-1,3,8-triazaspiro<4.5>decan-4-one

Base Information

Chemical Name:8-<3-propyl>-1-(4-chlorophenyl)-1,3,8-triazaspiro<4.5>decan-4-one
CAS No.:97861-00-2
Molecular Formula:C₂₈H₂₉ClF₂N₄O
Molecular Weight:511.014
Hs Code.:

8-<3-<bis(4-fluorophenyl)amino>propyl>-1-(4-chlorophenyl)-1,3,8-triazaspiro<4.5>decan-4-one

Synonyms:8-<3-propyl>-1-(4-chlorophenyl)-1,3,8-triazaspiro<4.5>decan-4-one

Suppliers and Price of 8-<3-propyl>-1-(4-chlorophenyl)-1,3,8-triazaspiro<4.5>decan-4-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-<3-propyl>-1-(4-chlorophenyl)-1,3,8-triazaspiro<4.5>decan-4-one

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Technology Process of 8-<3-propyl>-1-(4-chlorophenyl)-1,3,8-triazaspiro<4.5>decan-4-one

There total 6 articles about 8-<3-propyl>-1-(4-chlorophenyl)-1,3,8-triazaspiro<4.5>decan-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 97861-29-5
8-<3-propyl>-1-(4-chlorophenyl)-1,3,8-triazaspiro<4.5>dec-2-en-4-one

: 97861-00-2
8-<3-propyl>-1-(4-chlorophenyl)-1,3,8-triazaspiro<4.5>decan-4-one

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; under 2585.7 Torr;
DOI:10.1021/jm00150a011

Reference yield:

: 41979-39-9
4-piperidone hydrochloride

: 97861-00-2
8-<3-propyl>-1-(4-chlorophenyl)-1,3,8-triazaspiro<4.5>decan-4-one

Guidance literature:: Multi-step reaction with 5 steps

1: 67 percent / sodium carbonate, sodium iodide / dimethylformamide / 20 h / 75 - 90 °C

2: 1.) toluene, reflux, 2.5 h, 2.) toluene, 50 deg C

3: 85 percent / conc. sulfuric acid / 24 h / 25 °C

4: toluene / 48 h / Heating

5: 50 percent / H₂ / 5 percent Pd/C / methanol / 2585.7 Torr

With sulfuric acid; hydrogen; sodium carbonate; sodium iodide; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm00150a011

Reference yield:

: 80119-31-9
N-(3-chloropropyl)-4-fluoro-N-(4-fluorophenyl)benzenamine

: 97861-00-2
8-<3-propyl>-1-(4-chlorophenyl)-1,3,8-triazaspiro<4.5>decan-4-one

Guidance literature:: Multi-step reaction with 5 steps

1: 67 percent / sodium carbonate, sodium iodide / dimethylformamide / 20 h / 75 - 90 °C

2: 1.) toluene, reflux, 2.5 h, 2.) toluene, 50 deg C

3: 85 percent / conc. sulfuric acid / 24 h / 25 °C

4: toluene / 48 h / Heating

5: 50 percent / H₂ / 5 percent Pd/C / methanol / 2585.7 Torr

With sulfuric acid; hydrogen; sodium carbonate; sodium iodide; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm00150a011