4-(methylthio)phenyl bis<(E)-5-(2-bromovinyl)-2'-deoxyuridin-5'-yl> phosphate

Base Information

Chemical Name:4-(methylthio)phenyl bis<(E)-5-(2-bromovinyl)-2'-deoxyuridin-5'-yl> phosphate
CAS No.:125440-26-8
Molecular Formula:C₂₉H₃₁Br₂N₄O₁₂PS
Molecular Weight:850.432
Hs Code.:

Synonyms:4-(methylthio)phenyl bis<(E)-5-(2-bromovinyl)-2'-deoxyuridin-5'-yl> phosphate

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Chemical Property of 4-(methylthio)phenyl bis<(E)-5-(2-bromovinyl)-2'-deoxyuridin-5'-yl> phosphate

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Technology Process of 4-(methylthio)phenyl bis<(E)-5-(2-bromovinyl)-2'-deoxyuridin-5'-yl> phosphate

There total 3 articles about 4-(methylthio)phenyl bis<(E)-5-(2-bromovinyl)-2'-deoxyuridin-5'-yl> phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 125440-23-5
4-(methylthio)phenyl bis<(E)-5-(2-bromovinyl)-3'-O-acetyl-2'-deoxyuridin-5'-yl> phosphate

: 125440-26-8
4-(methylthio)phenyl bis<(E)-5-(2-bromovinyl)-2'-deoxyuridin-5'-yl> phosphate

Guidance literature:: With potassium carbonate; In methanol; water; Ambient temperature;
DOI:10.1021/jm00167a019

Reference yield:

: 1073-72-9
4-hydroxythioanisole

: 125440-26-8
4-(methylthio)phenyl bis<(E)-5-(2-bromovinyl)-2'-deoxyuridin-5'-yl> phosphate

Guidance literature:: Multi-step reaction with 3 steps

1: 42 percent / phosphoryl chloride, 1-methylimidazole / 20 h / Heating

2: 55 percent / 1-methylimidazole / acetonitrile / 20 h / Ambient temperature

3: 70 percent / potassium carbonate / methanol; H₂O / Ambient temperature

With 1-methyl-1H-imidazole; potassium carbonate; trichlorophosphate; In methanol; water; acetonitrile;
DOI:10.1021/jm00167a019

Reference yield:

: 53676-21-4
4-(methylthio)phenyl phosphorodichloridate

: 125440-26-8
4-(methylthio)phenyl bis<(E)-5-(2-bromovinyl)-2'-deoxyuridin-5'-yl> phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / 1-methylimidazole / acetonitrile / 20 h / Ambient temperature

2: 70 percent / potassium carbonate / methanol; H₂O / Ambient temperature

With 1-methyl-1H-imidazole; potassium carbonate; In methanol; water; acetonitrile;
DOI:10.1021/jm00167a019