C₁₇H₁₃ClN₄OS

Base Information

Chemical Name:C₁₇H₁₃ClN₄OS
CAS No.:1329990-81-9
Molecular Formula:C₁₇H₁₃ClN₄OS
Molecular Weight:356.835
Hs Code.:

C<sub>17</sub>H<sub>13</sub>ClN<sub>4</sub>OS

Synonyms:C₁₇H₁₃ClN₄OS

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Chemical Property of C₁₇H₁₃ClN₄OS

Chemical Property:

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Technology Process of C₁₇H₁₃ClN₄OS

There total 7 articles about C₁₇H₁₃ClN₄OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1329991-72-1
C₁₈H₁₄ClN₃O₃S₂

: 1329990-81-9
C₁₇H₁₃ClN₄OS

Guidance literature:: With ammonia; In isopropyl alcohol; at 50 ℃; for 0.5h;

Reference yield:

: 1329991-66-3
C₁₀H₁₁F₃N₂O₃S₂

: 1329990-81-9
C₁₇H₁₃ClN₄OS

Guidance literature:: Multi-step reaction with 7 steps

1: potassium carbonate; ethanol / 1 h / Reflux

2: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / 20 °C / Cooling with ice; Inert atmosphere

3: hydrogen / palladium 10% on activated carbon / isopropyl alcohol / 6 h / 20 °C

4: sodium hydride / pyridine; oil / 3 h / 50 °C / Cooling with ice

5: triethylamine / copper diacetate / dichloromethane / 1 h / Reflux

6: 3-chloro-benzenecarboperoxoic acid / chloroform / 0.75 h / Reflux

7: ammonia / isopropyl alcohol / 0.5 h / 50 °C

With ethanol; ammonia; hydrogen; sodium hexamethyldisilazane; sodium hydride; potassium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; palladium 10% on activated carbon; copper diacetate; In tetrahydrofuran; pyridine; dichloromethane; chloroform; isopropyl alcohol; oil;

Reference yield:

: 1329991-67-4
C₈H₁₂N₂O₂S₂

: 1329990-81-9
C₁₇H₁₃ClN₄OS

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / 20 °C / Cooling with ice; Inert atmosphere

2: hydrogen / palladium 10% on activated carbon / isopropyl alcohol / 6 h / 20 °C

3: sodium hydride / pyridine; oil / 3 h / 50 °C / Cooling with ice

4: triethylamine / copper diacetate / dichloromethane / 1 h / Reflux

5: 3-chloro-benzenecarboperoxoic acid / chloroform / 0.75 h / Reflux

6: ammonia / isopropyl alcohol / 0.5 h / 50 °C

With ammonia; hydrogen; sodium hexamethyldisilazane; sodium hydride; triethylamine; 3-chloro-benzenecarboperoxoic acid; palladium 10% on activated carbon; copper diacetate; In tetrahydrofuran; pyridine; dichloromethane; chloroform; isopropyl alcohol; oil;