TRANS-1,1,2,2,3,4-HEXAFLUOROCYCLOBUTANE

Base Information

• Chemical Name: TRANS-1,1,2,2,3,4-HEXAFLUOROCYCLOBUTANE
• CAS No.: 23012-94-4
• Molecular Formula: C₄H₂F₆
• Molecular Weight: 164.05
• Hs Code.: 2903890090
• Mol file: 23012-94-4.mol

Synonyms:Cyclobutane,1,1,2,2,3,4-hexafluoro-, trans- (8CI); trans-1,1,2,2,3,4-Hexafluorocyclobutane

Chemical Property of TRANS-1,1,2,2,3,4-HEXAFLUOROCYCLOBUTANE

Chemical Property:

• Vapor Pressure: 720.859mmHg at 25°C
• Refractive Index: 1.297
• Boiling Point: 26.5°Cat760mmHg
• Flash Point: °C
• PSA: 0.00000
• Density: 1.49g/cm³
• LogP: 1.94680

Purity/Quality:

98%min ^*data from raw suppliers

trans-1,1,2,2,3,4-Hexafluorocyclobutane ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

Useful:

Technology Process of TRANS-1,1,2,2,3,4-HEXAFLUOROCYCLOBUTANE

There total 7 articles about TRANS-1,1,2,2,3,4-HEXAFLUOROCYCLOBUTANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

1,2-dichloroperfluorocyclobutane (356-18-3) → cis-1,1,2,2,3,4-hexafluorocyclobutane (22819-47-2) + trans-1,2-dihydrohexafluorocyclobutane (377-95-7,22819-47-2,23012-94-4)

Guidance literature:

With tri-n-butyl-tin hydride; at 25 - 30 ℃; for 3h;

DOI:10.1016/0022-1139(94)03153-Q

Reference yield:

2,3,3-trifluoro-1-cyclobutene (3932-66-9) → 1,1,2,2,3,3-hexafluorocyclobutane (54572-23-5) + 1,1,2,2,3-Pentafluor-cyclobutan (2253-02-3) + cis-1,1,2,2,3,4-hexafluorocyclobutane (22819-47-2) + trans-1,1,2,2,3,4-hexafluorocyclobutane (377-95-7,22819-47-2,23012-94-4)

Guidance literature:

With cobalt (III) fluoride; at 100 ℃; for 24h; Further Variations:; Reagents; Temperatures; time; Product distribution;

DOI:10.1016/j.jfluchem.2005.10.007

Reference yield:

cis-1,2-dichloro-1,2,3,3,4,4-hexafluorocyclobutane (3934-26-7) → cis-1,1,2,2,3,4-hexafluorocyclobutane (22819-47-2) + trans-1,2-dihydrohexafluorocyclobutane (377-95-7,22819-47-2,23012-94-4)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether;

DOI:10.1039/jr9610003198

upstream raw materials:

3,3,4,4-tetrafluorocyclobutene

2,3,3-trifluoro-1-cyclobutene

1,2-dichloroperfluorocyclobutane

cis-1,2-dichloro-1,2,3,3,4,4-hexafluorocyclobutane

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