C₃₈H₅₅N₃

Base Information

• Chemical Name: C₃₈H₅₅N₃
• CAS No.: 174753-42-5
• Molecular Formula: C₃₈H₅₅N₃
• Molecular Weight: 553.875
• Mol file: 174753-42-5.mol

Synonyms:C₃₈H₅₅N₃

Chemical Property of C₃₈H₅₅N₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₃₈H₅₅N₃

There total 17 articles about C₃₈H₅₅N₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

C41H63N3Si (174753-38-9) → C38H55N3 (174753-42-5)

Guidance literature:

With methanol; potassium carbonate; at 23 ℃;

Reference yield:

1-(3'-aminophenyl)-3-ethylheptane (187871-17-6) → C38H55N3 (174753-42-5)

Guidance literature:

Multi-step reaction with 8 steps

1: 87 percent / 1 N NaOH / tetrahydrofuran / 2 h / Heating

2: AlCl₃ / CS₂ / 3 h / 70 °C

3: 3 N NaOH

4: 1.) t-BuONO, BF₃-OEt₂, 2.) K₂CO₃ / 1.) CH₂Cl₂, 0 deg C, 30 min, 2.) 1 h

6: 92 percent / MeI / 120 °C

7: 78 percent / Pd(dba)2, Ph₃P, CuI, i-Pr₂NH / tetrahydrofuran

8: 98 percent / TBAF / tetrahydrofuran

With sodium hydroxide; copper(l) iodide; aluminium trichloride; tert.-butylnitrite; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; potassium carbonate; diisopropylamine; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; methyl iodide; In tetrahydrofuran; carbon disulfide;

DOI:10.1021/jo962336q

Reference yield:

4-amino-2-(3'-ethylheptyl)acetophenone (187871-22-3) → C38H55N3 (174753-42-5)

Guidance literature:

Multi-step reaction with 5 steps

1: 1.) t-BuONO, BF₃-OEt₂, 2.) K₂CO₃ / 1.) CH₂Cl₂, 0 deg C, 30 min, 2.) 1 h

3: 92 percent / MeI / 120 °C

4: 78 percent / Pd(dba)2, Ph₃P, CuI, i-Pr₂NH / tetrahydrofuran

5: 98 percent / TBAF / tetrahydrofuran

With copper(l) iodide; tert.-butylnitrite; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; potassium carbonate; diisopropylamine; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; methyl iodide; In tetrahydrofuran;

DOI:10.1021/jo962336q

upstream raw materials:

C₄₁H₆₃N₃Si

2-Ethylhexyl alcohol

3-(iodomethyl)heptane

1-(3'-aminophenyl)-3-ethylheptane

Downstream raw materials:

C₇₅H₁₀₇N₃Si