ethyl 2-[(N-tert-butoxycarbonyl)-[[2'-[1-(triphenylmethyl)-1H-tetrazol-5-yl]biphenyl-4-yl]methyl]amino]-3-nitrobenzoate

Base Information

Chemical Name:ethyl 2-[(N-tert-butoxycarbonyl)-[[2'-[1-(triphenylmethyl)-1H-tetrazol-5-yl]biphenyl-4-yl]methyl]amino]-3-nitrobenzoate
CAS No.:906474-56-4
Molecular Formula:C₄₇H₄₂N₆O₆
Molecular Weight:786.887
Hs Code.:

Synonyms:ethyl 2-[(N-tert-butoxycarbonyl)-[[2'-[1-(triphenylmethyl)-1H-tetrazol-5-yl]biphenyl-4-yl]methyl]amino]-3-nitrobenzoate

Suppliers and Price of ethyl 2-[(N-tert-butoxycarbonyl)-[[2'-[1-(triphenylmethyl)-1H-tetrazol-5-yl]biphenyl-4-yl]methyl]amino]-3-nitrobenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ethyl 2-[(N-tert-butoxycarbonyl)-[[2'-[1-(triphenylmethyl)-1H-tetrazol-5-yl]biphenyl-4-yl]methyl]amino]-3-nitrobenzoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ethyl 2-[(N-tert-butoxycarbonyl)-[[2'-[1-(triphenylmethyl)-1H-tetrazol-5-yl]biphenyl-4-yl]methyl]amino]-3-nitrobenzoate

There total 1 articles about ethyl 2-[(N-tert-butoxycarbonyl)-[[2'-[1-(triphenylmethyl)-1H-tetrazol-5-yl]biphenyl-4-yl]methyl]amino]-3-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 136285-65-9
ethyl 2-[(N-tert-butoxycarbonyl)amino]-3-nitrobenzoate

: 124750-51-2
N-(triephenylmethyl)-5-<4'-(bromomethyl)-biphenyl-2-yl>tetrazole

: 906474-56-4
ethyl 2-[(N-tert-butoxycarbonyl)-[[2'-[1-(triphenylmethyl)-1H-tetrazol-5-yl]biphenyl-4-yl]methyl]amino]-3-nitrobenzoate

Guidance literature:: With potassium carbonate; In acetonitrile; for 5h; Reflux;
DOI:10.3987/COM-10-11944

Reference yield: 94.0%

: 906474-56-4
ethyl 2-[(N-tert-butoxycarbonyl)-[[2'-[1-(triphenylmethyl)-1H-tetrazol-5-yl]biphenyl-4-yl]methyl]amino]-3-nitrobenzoate

: 1073117-27-7
2-[(N-tert-butoxycarbonyl)-[[2'-[1-(triphenylmethyl)-1H-tetrazol-5-yl]biphenyl-4-yl]methyl]amino]-3-nitrobenzoic acid

Guidance literature:: With water; sodium hydroxide; In tetrahydrofuran; for 12h; Reflux;
DOI:10.3987/COM-10-11944

Reference yield:

: 906474-56-4
ethyl 2-[(N-tert-butoxycarbonyl)-[[2'-[1-(triphenylmethyl)-1H-tetrazol-5-yl]biphenyl-4-yl]methyl]amino]-3-nitrobenzoate

candesartan cilexetil: 145040-37-5
candesartan cilexetil

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydroxide / N,N-dimethyl acetamide / 2 h / 20 °C

2: potassium carbonate / N,N-dimethyl acetamide / 6 h / 60 °C

3: Raney Nickle / N,N-dimethyl acetamide / 24 h / 20 °C / 2625.26 Torr

4: hydrogenchloride / ethanol / 3 h / 20 °C

5: tetrahydrofuran / 6 h / 5 °C / Inert atmosphere

With hydrogenchloride; potassium carbonate; sodium hydroxide; In tetrahydrofuran; ethanol; N,N-dimethyl acetamide;