12-[2-(2-allyloxy-4-hydroxymethyl-phenoxy)-ethoxy]-3,8,13-trimethoxy-10,15-dihydro-5H-tribenzo[a,d,g]cyclononene-2,7-diol

Base Information

• Chemical Name: 12-[2-(2-allyloxy-4-hydroxymethyl-phenoxy)-ethoxy]-3,8,13-trimethoxy-10,15-dihydro-5H-tribenzo[a,d,g]cyclononene-2,7-diol
• CAS No.: 426821-82-1
• Molecular Formula: C₃₆H₃₈O₉
• Molecular Weight: 614.692

Synonyms:12-[2-(2-allyloxy-4-hydroxymethyl-phenoxy)-ethoxy]-3,8,13-trimethoxy-10,15-dihydro-5H-tribenzo[a,d,g]cyclononene-2,7-diol

Chemical Property of 12-[2-(2-allyloxy-4-hydroxymethyl-phenoxy)-ethoxy]-3,8,13-trimethoxy-10,15-dihydro-5H-tribenzo[a,d,g]cyclononene-2,7-diol

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of 12-[2-(2-allyloxy-4-hydroxymethyl-phenoxy)-ethoxy]-3,8,13-trimethoxy-10,15-dihydro-5H-tribenzo[a,d,g]cyclononene-2,7-diol

There total 1 articles about 12-[2-(2-allyloxy-4-hydroxymethyl-phenoxy)-ethoxy]-3,8,13-trimethoxy-10,15-dihydro-5H-tribenzo[a,d,g]cyclononene-2,7-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

cyclotriguaiacyclene (81370-49-2,68198-62-9,75322-24-6,68182-93-4) + [3-allyloxy-4-(2-iodoethoxy)phenyl]methanol (426821-81-0) → 12-[2-(2-allyloxy-4-hydroxymethyl-phenoxy)-ethoxy]-3,8,13-trimethoxy-10,15-dihydro-5H-tribenzo[a,d,g]cyclononene-2,7-diol (426821-82-1)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 18h;

DOI:10.1039/b109301k

Reference yield: 80.0%

2-[4-(2-iodoethoxy)-3-methoxybenzyloxy]-tetrahydropyran (347894-43-3) + 12-[2-(2-allyloxy-4-hydroxymethyl-phenoxy)-ethoxy]-3,8,13-trimethoxy-10,15-dihydro-5H-tribenzo[a,d,g]cyclononene-2,7-diol (426821-82-1) → {3-allyloxy-4-[2-(3,8,13-trimethoxy-7,12-bis-{2-[2-methoxy-4-(tetrahydro-pyran-2-yloxymethyl)-phenoxy]-ethoxy}-10,15-dihydro-5H-tribenzo[a,d,g]cyclononen-2-yloxy)-ethoxy]-phenyl}-methanol (391895-30-0)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 18h;

DOI:10.1039/b109301k

upstream raw materials:

cyclotriguaiacyclene

[3-allyloxy-4-(2-iodoethoxy)phenyl]methanol

Downstream raw materials:

{3-allyloxy-4-[2-(3,8,13-trimethoxy-7,12-bis-{2-[2-methoxy-4-(tetrahydro-pyran-2-yloxymethyl)-phenoxy]-ethoxy}-10,15-dihydro-5H-tribenzo[a,d,g]cyclononen-2-yloxy)-ethoxy]-phenyl}-methanol

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