5--N-<2-(methoxycarbonyl)ethyl>-2,4-dinitrobenzamide

Base Information

Chemical Name:5--N-<2-(methoxycarbonyl)ethyl>-2,4-dinitrobenzamide
CAS No.:150272-13-2
Molecular Formula:C₁₅H₁₈Cl₂N₄O₇
Molecular Weight:437.237
Hs Code.:

5-<N,N-bis(2-chloroethyl)amino>-N-<2-(methoxycarbonyl)ethyl>-2,4-dinitrobenzamide

Synonyms:5--N-<2-(methoxycarbonyl)ethyl>-2,4-dinitrobenzamide

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Chemical Property of 5--N-<2-(methoxycarbonyl)ethyl>-2,4-dinitrobenzamide

Chemical Property:

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Technology Process of 5--N-<2-(methoxycarbonyl)ethyl>-2,4-dinitrobenzamide

There total 6 articles about 5--N-<2-(methoxycarbonyl)ethyl>-2,4-dinitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4138-35-6
methyl 3-aminopropanoate

: 156423-11-9
5--2,4-dinitrobenzoyl chloride

: 150272-13-2
5--N-<2-(methoxycarbonyl)ethyl>-2,4-dinitrobenzamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1021/jm00040a009

Reference yield:

: 150272-08-5
methyl 5-chloro-2,4-dinitrobenzoate

: 150272-13-2
5--N-<2-(methoxycarbonyl)ethyl>-2,4-dinitrobenzamide

Guidance literature:: Multi-step reaction with 6 steps

1: 97 percent / dioxane / 3 h / 50 °C

2: Et₃N / CH₂Cl₂ / 0.25 h / 0 °C

3: LiCl / dimethylformamide / 0.01 h / 120 °C

4: 100 percent / 4 n aq. KOH / dioxane / 0.25 h / 20 °C

5: SOCl₂, DMF / 0.33 h / Heating

6: Et₃N / CH₂Cl₂ / 2 h / 20 °C

With potassium hydroxide; thionyl chloride; triethylamine; N,N-dimethyl-formamide; lithium chloride; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00040a009

Reference yield:

: 150271-91-3
SN 24939

: 150272-13-2
5--N-<2-(methoxycarbonyl)ethyl>-2,4-dinitrobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂, DMF / 0.33 h / Heating

2: Et₃N / CH₂Cl₂ / 2 h / 20 °C

With thionyl chloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1021/jm00040a009