Technology Process of C24H41NO3
There total 7 articles about C24H41NO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C24H39NO2;
With
dimethylsulfide borane complex;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 3h;
With
sodium hydroxide; dihydrogen peroxide;
at 0 - 20 ℃;
for 6h;
Further stages.;
DOI:10.1055/s-2007-991056
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: 41 percent / H2O / (R,R)-Co(III)(salen)*OAc / 24 h / 0 °C
2.1: 94 percent / CuI / tetrahydrofuran / 12 h / -78 °C
3.1: Et3N / CH2Cl2 / 2 h
4.1: NaN3 / dimethylformamide / 45 °C
5.1: PPh3 / tetrahydrofuran; H2O / 12 h / 20 °C
6.1: Na2CO3 / dioxane; H2O / 0 - 20 °C
7.1: BH3*SMe2 / tetrahydrofuran / 3 h / 0 - 20 °C
7.2: 87 percent / NaOH; H2O2 / 6 h / 0 - 20 °C
With
copper(l) iodide; sodium azide; dimethylsulfide borane complex; water; sodium carbonate; triethylamine; triphenylphosphine;
(R,R)-Co(III)(salen)*OAc;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide;
1.1: Jacobsen's hydrolytic kinetic resolution / 5.1: Staudinger reaction;
DOI:10.1055/s-2007-991056
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: NaN3 / dimethylformamide / 45 °C
2.1: PPh3 / tetrahydrofuran; H2O / 12 h / 20 °C
3.1: Na2CO3 / dioxane; H2O / 0 - 20 °C
4.1: BH3*SMe2 / tetrahydrofuran / 3 h / 0 - 20 °C
4.2: 87 percent / NaOH; H2O2 / 6 h / 0 - 20 °C
With
sodium azide; dimethylsulfide borane complex; sodium carbonate; triphenylphosphine;
In
tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide;
2.1: Staudinger reaction;
DOI:10.1055/s-2007-991056
