2,3-Diiodopyridine

Base Information

Chemical Name:2,3-Diiodopyridine
CAS No.:83674-70-8
Molecular Formula:C5H3I2N
Molecular Weight:330.895
Hs Code.:2933399090
European Community (EC) Number:804-610-5
DSSTox Substance ID:DTXSID70509151
Nikkaji Number:J3.627.546D
Wikidata:Q82366534
Mol file:83674-70-8.mol

Synonyms:2,3-Diiodopyridine;83674-70-8;2,3-Diiodo-pyridine;diiodopyridine;2,3-bis(iodanyl)pyridine;SCHEMBL503888;DTXSID70509151;2,3-Diiodo-pyridine, AldrichCPR;MFCD06658996;AKOS015853950;AB25846;BS-22792;FT-0659393;E90003;A840631

Suppliers and Price of 2,3-Diiodopyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

SynQuest Laboratories
2,3-Diiodopyridine
5 g
$ 1432.00

SynQuest Laboratories
2,3-Diiodopyridine
1 g
$ 464.00

Sigma-Aldrich
2,3-Diiodo-pyridine Aldrich
1g
$ 168.00

Matrix Scientific
2,3-Diiodopyridine
1g
$ 239.00

Matrix Scientific
2,3-Diiodopyridine
500mg
$ 155.00

Crysdot
2,3-Diiodopyridine 95+%
5g
$ 677.00

Apolloscientific
2,3-Diiodopyridine
5g
$ 1298.00

Apolloscientific
2,3-Diiodopyridine
1g
$ 421.00

AOBChem
2,3-Diiodopyridine 95%
10g
$ 656.00

AOBChem
2,3-Diiodopyridine 95%
5g
$ 385.00

Total 19 raw suppliers

Chemical Property of 2,3-Diiodopyridine

Chemical Property:

Vapor Pressure:0.001mmHg at 25°C
Melting Point:64.7-64.9 °C
Refractive Index:1.721
Boiling Point:305.303 °C at 760 mmHg
Flash Point:138.443 °C
PSA：12.89000
Density:2.609 g/cm³
LogP:2.29080
Storage Temp.:under inert gas (nitrogen or Argon) at 2–8 °C
XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:330.83549
Heavy Atom Count:8
Complexity:76.8

Purity/Quality:

97% ^*data from raw suppliers

2,3-Diiodopyridine ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi,Xn
Statements: 22-37/38-41
Safety Statements: 26-39

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(N=C1)I)I

Technology Process of 2,3-Diiodopyridine

There total 1 articles about 2,3-Diiodopyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13534-89-9
2,3-dibromopyridine

: 83674-70-8
2,3-diiodopyridine

Guidance literature:: With trimethylstannylsodium; iodine; Yield given. Multistep reaction; 1.) DME, 3 h, cooling 2.) THF, 1 h, room temp.;

Reference yield: 95.0%

: 83674-70-8
2,3-diiodopyridine

: 536-74-3
phenylacetylene

: 1392013-91-0
2,3-bis(phenylethynyl)pyridine

Guidance literature:: 2,3-diiodopyridine; With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In N,N-dimethyl-formamide; Inert atmosphere;

phenylacetylene; In N,N-dimethyl-formamide; at 65 ℃; Inert atmosphere;
DOI:10.1039/c5ra21701f

Reference yield: 72.0%

: 83674-70-8
2,3-diiodopyridine

: 536-74-3
phenylacetylene

: 1392013-91-0
2,3-bis(phenylethynyl)pyridine

: 1629167-75-4
3-iodo-2-(phenylethynyl)pyridine

Guidance literature:: 2,3-diiodopyridine; With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In N,N-dimethyl-formamide; Inert atmosphere;

phenylacetylene; In N,N-dimethyl-formamide; at 65 ℃; Inert atmosphere;
DOI:10.1039/c5ra21701f