diphenylthiophosphinic acid-S-naphthalene-1-ester

Base Information

• Chemical Name: diphenylthiophosphinic acid-S-naphthalene-1-ester
• CAS No.: 5510-82-7
• Molecular Formula: C₂₂H₁₇OPS
• Molecular Weight: 360.416
• Mol file: 5510-82-7.mol

Synonyms:diphenylthiophosphinic acid-S-naphthalene-1-ester

Chemical Property of diphenylthiophosphinic acid-S-naphthalene-1-ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of diphenylthiophosphinic acid-S-naphthalene-1-ester

There total 5 articles about diphenylthiophosphinic acid-S-naphthalene-1-ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

1-Naphthalenesulfonyl chloride (85-46-1) + Diphenylphosphine oxide (4559-70-0) → diphenylthiophosphinic acid-S-naphthalene-1-ester (5510-82-7)

Guidance literature:

In acetonitrile; at 20 ℃; for 5h; Green chemistry;

DOI:10.1016/j.tet.2016.10.012

Reference yield: 90.0%

1-Naphthalenethiol (529-36-2) + Diphenylphosphine oxide (4559-70-0) → diphenylthiophosphinic acid-S-naphthalene-1-ester (5510-82-7)

Guidance literature:

With lithium tert-butoxide; In chloroform; at 25 ℃; for 0.5h;

DOI:10.1039/c5ra16015d

Reference yield: 71.0%

N-(naphthalen-1-ylsulfanyl)succinimide + Diphenylphosphine oxide (4559-70-0) → diphenylthiophosphinic acid-S-naphthalene-1-ester (5510-82-7)

Guidance literature:

In water; at 40 ℃; for 2h;

upstream raw materials:

1-Naphthalenethiol

Diphenylphosphine oxide

1-Naphthalenesulfonyl chloride

chloro-diphenylphosphine