N-<2-<3,4-bis(benzyloxy)-5-(trifluoromethyl)phenyl>ethyl>-3',4',5'-trimethoxyphenylacetamide

Base Information

Chemical Name:N-<2-<3,4-bis(benzyloxy)-5-(trifluoromethyl)phenyl>ethyl>-3',4',5'-trimethoxyphenylacetamide
CAS No.:132335-32-1
Molecular Formula:C₃₄H₃₄F₃NO₆
Molecular Weight:609.642
Hs Code.:

Synonyms:N-<2-<3,4-bis(benzyloxy)-5-(trifluoromethyl)phenyl>ethyl>-3',4',5'-trimethoxyphenylacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<2-<3,4-bis(benzyloxy)-5-(trifluoromethyl)phenyl>ethyl>-3',4',5'-trimethoxyphenylacetamide

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Technology Process of N-<2-<3,4-bis(benzyloxy)-5-(trifluoromethyl)phenyl>ethyl>-3',4',5'-trimethoxyphenylacetamide

There total 5 articles about N-<2-<3,4-bis(benzyloxy)-5-(trifluoromethyl)phenyl>ethyl>-3',4',5'-trimethoxyphenylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 951-82-6
3,4,5-trimethoxyphenyl acetic acid

: 138491-29-9
2-(3,4-Bis-benzyloxy-5-trifluoromethyl-phenyl)-ethylamine

: 132335-32-1
N-<2-<3,4-bis(benzyloxy)-5-(trifluoromethyl)phenyl>ethyl>-3',4',5'-trimethoxyphenylacetamide

Guidance literature:: In toluene; for 72h; Heating;
DOI:10.1021/jm00081a007

Reference yield:

: 138491-23-3
3,4-dihydroxy-5-(trifluoromethyl)benzyl cyanide

: 132335-32-1
N-<2-<3,4-bis(benzyloxy)-5-(trifluoromethyl)phenyl>ethyl>-3',4',5'-trimethoxyphenylacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / potassium carbonate, potassium iodide / acetone / 5 h / Heating

2: 1 M diborane / tetrahydrofuran / 18 h / Heating

3: 79 percent / toluene / 72 h / Heating

With potassium carbonate; potassium iodide; diborane; In tetrahydrofuran; acetone; toluene;
DOI:10.1021/jm00081a007

Reference yield:

: 138491-21-1
4-hydroxy-3-methoxy-5-(trifluoromethyl)benzyl cyanide

: 132335-32-1
N-<2-<3,4-bis(benzyloxy)-5-(trifluoromethyl)phenyl>ethyl>-3',4',5'-trimethoxyphenylacetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / 1 M boron tribromide / CH₂Cl₂ / Ambient temperature

2: 82 percent / potassium carbonate, potassium iodide / acetone / 5 h / Heating

3: 1 M diborane / tetrahydrofuran / 18 h / Heating

4: 79 percent / toluene / 72 h / Heating

With boron tribromide; potassium carbonate; potassium iodide; diborane; In tetrahydrofuran; dichloromethane; acetone; toluene;
DOI:10.1021/jm00081a007