Benzyl N--L-prolinate

Base Information

Chemical Name:Benzyl N--L-prolinate
CAS No.:136583-36-3
Molecular Formula:C₂₂H₂₈N₂O₄
Molecular Weight:384.475
Hs Code.:

Benzyl N-<N-Acetyl-2,2-bis(prop-2-en-1-yl)glycyl>-L-prolinate

Synonyms:Benzyl N--L-prolinate

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Chemical Property of Benzyl N--L-prolinate

Chemical Property:

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Technology Process of Benzyl N--L-prolinate

There total 3 articles about Benzyl N--L-prolinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 108-24-7
acetic anhydride

: 136583-26-1
Benzyl N-<2-Nitro-2,2-bis(prop-2-en-1-yl)acetyl>-L-prolinate

: 136583-36-3
Benzyl N--L-prolinate

Guidance literature:: With acetic acid; zinc; at 40 - 60 ℃;
DOI:10.1002/hlca.19910740516

Reference yield:

: 134038-38-3
N-nitroacetyl(L)-proline benzyl ester

: 136583-36-3
Benzyl N--L-prolinate

Guidance literature:: Multi-step reaction with 3 steps

1: 1) 1,8-diazabicyclo<5.4.0>undec-7-ene, bis(dibenzylidene)palladium⁽⁰⁾, PPh₃ / 1) MeCN, 5 min; 2) MeCN, 25-30 deg C, 8-10 h

2: 1) 1,8-diazabicyclo<5.4.0>undec-7-ene, bis(dibenzylidene)palladium⁽⁰⁾, PPh₃ / 1) MeCN, 5 min; 2) MeCN, 25-30 deg C, 8-10 h

3: 75 percent / Zn, HOAc / 40 - 60 °C

With acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; zinc;
DOI:10.1002/hlca.19910740516

Reference yield:

: 134038-47-4,134038-48-5
Benzyl N-<2-Nitro-2-(prop-2-en-1-yl)acetyl>-L-prolinate

: 136583-36-3
Benzyl N--L-prolinate

Guidance literature:: Multi-step reaction with 2 steps

1: 1) 1,8-diazabicyclo<5.4.0>undec-7-ene, bis(dibenzylidene)palladium⁽⁰⁾, PPh₃ / 1) MeCN, 5 min; 2) MeCN, 25-30 deg C, 8-10 h

2: 75 percent / Zn, HOAc / 40 - 60 °C

With acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; zinc;
DOI:10.1002/hlca.19910740516