C₃₀H₅₈O₄Si₂

Base Information

Chemical Name:C₃₀H₅₈O₄Si₂
CAS No.:944052-11-3
Molecular Formula:C₃₀H₅₈O₄Si₂
Molecular Weight:538.959
Hs Code.:

C<sub>30</sub>H<sub>58</sub>O<sub>4</sub>Si<sub>2</sub>

Synonyms:C₃₀H₅₈O₄Si₂

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Chemical Property of C₃₀H₅₈O₄Si₂

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Technology Process of C₃₀H₅₈O₄Si₂

There total 11 articles about C₃₀H₅₈O₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 944052-27-1
C₃₆H₇₂O₄Si₃

: 944052-11-3
C₃₀H₅₈O₄Si₂

Guidance literature:: With pyridine; hydrogen fluoride; In tetrahydrofuran; at 0 - 20 ℃; for 5h;
DOI:10.1016/j.tetlet.2007.04.016

Reference yield:

: C₃₂H₄₄O₄Si

: 944052-11-3
C₃₀H₅₈O₄Si₂

Guidance literature:: Multi-step reaction with 11 steps

1: 98 percent / CSA / CH₂Cl₂ / 0 - 20 °C

2: 78 percent / Li; liq. NH₃ / tetrahydrofuran / 0.17 h / -33 °C

3: 70 percent / Et₃N; DMAP / CH₂Cl₂ / 0 - 20 °C

4: 92 percent / TBAF / tetrahydrofuran / 0 - 20 °C

5: (COCl)2; DMSO; Et₃N / CH₂Cl₂ / 2 h / -78 - 0 °C

6: CH₂Cl₂ / 20 °C

7: 86 percent / LiBH₄ / tetrahydrofuran / 16 h / 0 - 20 °C

8: 96 percent / NaHMDS / tetrahydrofuran; dimethylformamide / 0 - 20 °C

9: 65 percent / TFA / 2-methyl-propan-2-ol / 2 h / 20 °C

10: 100 percent / 2,6-lutidine / 0.17 h / 0 °C

11: 75 percent / HF; pyridine / tetrahydrofuran / 5 h / 0 - 20 °C

With pyridine; 2,6-dimethylpyridine; dmap; lithium borohydride; oxalyl dichloride; camphor-10-sulfonic acid; hydrogen fluoride; tetrabutyl ammonium fluoride; ammonia; sodium hexamethyldisilazane; lithium; dimethyl sulfoxide; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2007.04.016

Reference yield:

: 944052-04-4
C₃₅H₄₈O₄Si

: 944052-11-3
C₃₀H₅₈O₄Si₂

Guidance literature:: Multi-step reaction with 10 steps

1: 78 percent / Li; liq. NH₃ / tetrahydrofuran / 0.17 h / -33 °C

2: 70 percent / Et₃N; DMAP / CH₂Cl₂ / 0 - 20 °C

3: 92 percent / TBAF / tetrahydrofuran / 0 - 20 °C

4: (COCl)2; DMSO; Et₃N / CH₂Cl₂ / 2 h / -78 - 0 °C

5: CH₂Cl₂ / 20 °C

6: 86 percent / LiBH₄ / tetrahydrofuran / 16 h / 0 - 20 °C

7: 96 percent / NaHMDS / tetrahydrofuran; dimethylformamide / 0 - 20 °C

8: 65 percent / TFA / 2-methyl-propan-2-ol / 2 h / 20 °C

9: 100 percent / 2,6-lutidine / 0.17 h / 0 °C

10: 75 percent / HF; pyridine / tetrahydrofuran / 5 h / 0 - 20 °C

With pyridine; 2,6-dimethylpyridine; dmap; lithium borohydride; oxalyl dichloride; hydrogen fluoride; tetrabutyl ammonium fluoride; ammonia; sodium hexamethyldisilazane; lithium; dimethyl sulfoxide; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2007.04.016