(η5-cyclopentadienyl)cobalt{(phenyl)(dicarbomethoxy)(OCH3)-oxanorbornadiene}

Base Information Edit

Chemical Name:(η5-cyclopentadienyl)cobalt{(phenyl)(dicarbomethoxy)(OCH3)-oxanorbornadiene}
CAS No.:113158-74-0
Molecular Formula:C₂₁H₂₁CoO₆
Molecular Weight:428.387
Hs Code.:
Mol file:113158-74-0.mol

Synonyms:(η5-cyclopentadienyl)cobalt{(phenyl)(dicarbomethoxy)(OCH3)-oxanorbornadiene}

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (η5-cyclopentadienyl)cobalt{(phenyl)(dicarbomethoxy)(OCH3)-oxanorbornadiene} Edit

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MSDS Files:: SDS file from LookChem

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Technology Process of (η5-cyclopentadienyl)cobalt{(phenyl)(dicarbomethoxy)(OCH3)-oxanorbornadiene}

There total 10 articles about (η5-cyclopentadienyl)cobalt{(phenyl)(dicarbomethoxy)(OCH3)-oxanorbornadiene} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 53559-30-1
(η5-C5H5)Co{C(C6H5)=C(CO2CH3)CH(CO2CH3)CH(-cyclo-Co)(CO2CH3)}{P(C6H5)3}

: 113158-74-0
(η5-cyclopentadienyl)cobalt{(phenyl)(dicarbomethoxy)(OCH3)-oxanorbornadiene}

Guidance literature:: With silver trifluoromethanesulfonate; In benzene; reacted for 48 h under nitrogen atmosphere; concd., purified by column chromy. on SiO2 (eluent CH2Cl2-THF), recrystd. from benzene-hexane;
DOI:10.1021/om00147a015

Reference yield: 21.0%

: 10544-50-0
sulfur

: 53559-30-1
(η5-C5H5)Co{C(C6H5)=C(CO2CH3)CH(CO2CH3)CH(-cyclo-Co)(CO2CH3)}{P(C6H5)3}

: 113158-74-0
(η5-cyclopentadienyl)cobalt{(phenyl)(dicarbomethoxy)(OCH3)-oxanorbornadiene}

: 3878-45-3
triphenylphosphine sulfide

Guidance literature:: In benzene; mixt. of Co-complex, elemental sulfur, and benzene in a Schlenk flask was gradually warmed over the course of 0.5 h to 60°C under a nitrogen atmosphere; concd. under reduced pressure, sepd. by column chromy. on alumina (eluent benzene-ethyl acetate), Co-complex was recrystd. from benzene-hexane; elem. anal. for Co-complex;
DOI:10.1021/om00147a015