C₃₂H₄₄F₂N₆O₄Si

Base Information

Chemical Name:C₃₂H₄₄F₂N₆O₄Si
CAS No.:1202760-77-7
Molecular Formula:C₃₂H₄₄F₂N₆O₄Si
Molecular Weight:642.821
Hs Code.:

C<sub>32</sub>H<sub>44</sub>F<sub>2</sub>N<sub>6</sub>O<sub>4</sub>Si

Synonyms:C₃₂H₄₄F₂N₆O₄Si

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Chemical Property of C₃₂H₄₄F₂N₆O₄Si

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Technology Process of C₃₂H₄₄F₂N₆O₄Si

There total 12 articles about C₃₂H₄₄F₂N₆O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.6%

: 1202760-75-5
C₃₂H₄₂F₂N₆O₆Si

: 1202760-77-7
C₃₂H₄₄F₂N₆O₄Si

Guidance literature:: With hydrogen; palladium on activated carbon; In methanol; at 20 ℃; for 16h;

Reference yield:

: 40216-83-9
L-4-hydroxyproline methyl ester hydrochloride

: 1202760-77-7
C₃₂H₄₄F₂N₆O₄Si

Guidance literature:: Multi-step reaction with 7 steps

1: triethylamine / dichloromethane / 5 h / 20 °C

2: 1H-imidazole / N,N-dimethyl-formamide / 16 h

3: lithium aluminium tetrahydride / tetrahydrofuran / 0.25 h / -20 °C

4: di-isopropyl azodicarboxylate; triethylamine; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

5: hydrogen / palladium on activated carbon / methanol / 16 h / 20 °C

6: caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / palladium diacetate / toluene / 16 h / 110 °C / Inert atmosphere

7: hydrogen / palladium on activated carbon / methanol / 16 h / 20 °C

With 1H-imidazole; lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; hydrogen; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; triphenylphosphine; palladium on activated carbon; palladium diacetate; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1202760-77-7
C₃₂H₄₄F₂N₆O₄Si

Guidance literature:: Multi-step reaction with 7 steps

1: triethylamine / dichloromethane / 5 h / 20 °C

2: 1H-imidazole / N,N-dimethyl-formamide / 16 h

3: lithium aluminium tetrahydride / tetrahydrofuran / 0.25 h / -20 °C

4: di-isopropyl azodicarboxylate; triethylamine; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

5: hydrogen / palladium on activated carbon / methanol / 16 h / 20 °C

6: caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / palladium diacetate / toluene / 16 h / 110 °C / Inert atmosphere

7: hydrogen / palladium on activated carbon / methanol / 16 h / 20 °C

With 1H-imidazole; lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; hydrogen; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; triphenylphosphine; palladium on activated carbon; palladium diacetate; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;