hexyldiphenylbismutane

Base Information

Chemical Name:hexyldiphenylbismutane
CAS No.:74724-77-9
Molecular Formula:C₁₈H₂₃Bi
Molecular Weight:448.361
Hs Code.:

Synonyms:hexyldiphenylbismutane

Suppliers and Price of hexyldiphenylbismutane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of hexyldiphenylbismutane

Chemical Property:

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Technology Process of hexyldiphenylbismutane

There total 1 articles about hexyldiphenylbismutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 21369-64-2
n-hexyllithium

: 5153-28-6
diphenylbismuth(III) chloride

: 74724-77-9
hexyldiphenylbismutane

Guidance literature:: In diethyl ether; pentane; byproducts: LiCl, C6H5Bi((CH2)5CH3)2; react. under N2 in dry, N2-satd. solvents; dropwise addn. of Li-compd. in pentane to a stirred suspn. of Bi-compd. in ether (-70 to -65°C, 1 h), stirring for 0.5 h at -70°C, warming to room temp.; evapn. (vac.), reslurring of residue with benzine and decantation (3 times), evapn. of combined solns. (room temp., vac.), distn. of oily bismutane at 1E-1 to 1E-2 Torr; elem. anal.;